Microstructure of nanocrystalline powders of nonstoichiometric vanadium VC0.875 and niobium NbC0.93 carbides

被引:0
作者
Kurlov A.S. [1 ]
Balagurov A.M. [2 ]
Bobrikov I.A. [2 ]
Gusev A.I. [1 ]
机构
[1] Institute of Solid State Chemistry, Ural Branch, Russian Academy of Sciences, Yekaterinburg
[2] Joint Institute for Nuclear Research, Dubna, Moscow region
来源
Journal of Surface Investigation | 2016年 / 10卷 / 06期
关键词
microstructure; nanostructured carbides; neutron diffraction; nonstoichiometry;
D O I
10.1134/S1027451016050530
中图分类号
学科分类号
摘要
The evolution of the microstructure of nonstoichiometric vanadium VC0.875 and niobium NbC0.93 carbide powders subjected to high-energy ball milling is investigated by neutron diffraction. It is established that milling produces non uniform powders and two distinct fractions with differing microstructure can be identified in them. It is shown that the time-of-flight neutron-diffraction technique is promising for studying the microstructure of highly deformed nonstoichiometric carbides and for quantitative determination of the anisotropy of microstrains. © 2016, Pleiades Publishing, Ltd.
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页码:1136 / 1142
页数:6
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