Chemical and electrochemical synthesis, local atomic structure, and properties of copper(II), cobalt(II), and nickel(II) complexes with azo compounds containing an additional azo group in the para or ortho position of the amine fragment

被引：0
作者：
A. S. Burlov
S. A. Mashchenko
V. G. Vlasenko
E. D. Garnovskaya
Ya. V. Zubavichus
S. I. Levchenkov
Yu. S. Kurinnaya
机构：
[1] Southern Federal University,Research Institute of Physical and Organic Chemistry
[2] Southern Federal University,Research Institute of Physics
[3] “Kurchatov Institute” National Research Center,Southern Scientific Center
[4] Russian Academy of Sciences,undefined
来源：
Russian Journal of General Chemistry | 2015年 / 85卷
关键词：
azo compounds; metal chelates; X-ray absorption spectroscopy; local atomic structure; magnetochemistry; quantum chemical calculations;
D O I：
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中图分类号：
学科分类号：
摘要：
New copper(II), cobalt(II), and nickel(II) complexes with 1-[4-(phenydiazenyl)phenyldiazenyl]-naphthalen-2-ol and 1-[4-methyl-2-(4-methylphenyldiazenyl)phenyldiazenyl]naphthalen-2-ol have been synthesized by chemical and electrochemical methods and characterized by IR, 1H NMR, and X-ray absorption spectroscopy, as well as by magnetochemistry and quantum chemical calculations. Coordination of the nitrogen atom in the additional azo group to the metal ion is determined by its position (ortho or para) and metal nature.
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页码：2338 / 2347
页数：9
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