Phenolic-iodine Redox Products: Mass Spectrometry, Thermal and Other Physico-chemical Methods of Analyses

被引：0
作者：
M. A. Fahmey
M. A. Zayed
机构：
[1] N.R.C.,Nuclear Physics Department
[2] Atomic Energy Authority,Chemistry Department, Faculty of Science
[3] Cairo University,undefined
来源：
Journal of Thermal Analysis and Calorimetry | 2002年 / 67卷
关键词：
mass spectrometry; redox reactions; thermal analysis;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Three interesting new compounds formed as a result of phenols-iodine redox reactions were investigated by mass spectral fragmentation (MS) and thermal analyses (TA) as well as some other physicochemical methods as microanalysis and infra-red spectroscopy to elucidate their structures. The characterization of the compounds was satisfactorily achieved by using the above analytical tools and their proposed general formulae, were found to be C24H15O8I (PC-IO 3−), C24H14O12 I2 (PG-IO 3−) and C12H8O6I2 (PG-IO 4−).
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页码：163 / 175
页数：12
相关论文
共 28 条
  • [1] Mann M.(1995)undefined Trends Biochem. Sci. 20 219-undefined
  • [2] Wilm M.(1990)undefined Anal. Chem. 62 882-undefined
  • [3] Smith R. D.(1994)undefined J. Lipid. Res. 35 1102-undefined
  • [4] Loo J. A.(1996)undefined J. Am. Soc. Mass Spectrom. 7 140-undefined
  • [5] Edmonds C. G.(1995)undefined Meth. Enzymol. 250 614-undefined
  • [6] Barinaga C. J.(1995)undefined Anal. Chem. 67 1772-undefined
  • [7] Udseth H. R.(1997)undefined Rapid Comm. Mass Spectrom. 11 557-undefined
  • [8] Kerwin J. L.(1992)undefined J. Instrumental Analysis 11 18-undefined
  • [9] Tuininga A. R.(1987)undefined Thermochim. Acta 111 103-undefined
  • [10] Ericsson L. H.(1991)undefined Egypt. J. Chem. 84 371-undefined
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