Effect of Slurry Solid phase Content on the Process and Properties of Gel Injection Moulding Ti10Mo28Nb3Zr Alloy

被引:0
作者
Wu, Z. [1 ]
Xu, Y. [1 ]
Zhao, S. [1 ]
Cai, Y. [1 ]
Lou, B. [1 ]
机构
[1] North China Univ Sci & Technol, Coll Mat Sci & Engn, Key Lab Inorgan Nonmet Mat Hebei Prov, Tangshan 063009, Peoples R China
关键词
gel injection mold; titanium alloy; microwave sintering; solid phase content; performance; MECHANICAL-PROPERTIES; TITANIUM;
D O I
10.1134/S1990793124010378
中图分类号
O64 [物理化学(理论化学)、化学物理学]; O56 [分子物理学、原子物理学];
学科分类号
070203 ; 070304 ; 081704 ; 1406 ;
摘要
In order to solve the problems of high elastic modulus and biotoxicity of human bone implants, Ti10Mo28Nb3Zr, a component with low elastic modulus that had been calculated and verified by first-principles experiments, was used as raw material to prepare bone implant titanium alloy with low elastic modulus and good biocompatibility by means of gel injection and microwave sintering methods. The effects of solid content on gel curing time, shrinkage, porosity, compressive strength and elastic modulus of the materials were analyzed by scanning electron microscope, X-ray diffraction, metallographic microscope and compression tests. When the solid phase content increases from 30 to 45%, the gel time reduces from 300 to 205 s. This indicates that a higher solid phase content results in a shorter gel curing time. Meanwhile, the axial shrinkage decreased from 13.67 to 6.43%, and the radial shrinkage decreased from 13.11 to 6.18%. Moreover, the compressive strength increased from 125 to 215 MPa, the elastic modulus increased from 10.46 to 25.11 GPa. The results provide a basis for the preparation of medical bio-titanium alloy by gel injection molding and its application in bone implant materials.
引用
收藏
页码:101 / 110
页数:10
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