High throughput exploration of process-property linkages in Al-6061 using instrumented spherical microindentation and microstructurally graded samples

被引:58
作者
Weaver J.S. [1 ,2 ]
Khosravani A. [1 ]
Castillo A. [1 ]
Kalidindi S.R. [1 ]
机构
[1] George W. Woodruff School of Mechanical Engineering, Georgia Institute of Technology, Atlanta, GA
[2] Center for Integrated Nanotechnologies, Los Alamos National Laboratory, Los Alamos, NM
关键词
Aging; Al alloys; Hertzian indentation; High throughput; Sample libraries;
D O I
10.1186/s40192-016-0054-3
中图分类号
学科分类号
摘要
Recent spherical nanoindentation protocols have proven robust at capturing the local elastic-plastic response of polycrystalline metal samples at length scales much smaller than the grain size. In this work, we extend these protocols to length scales that include multiple grains to recover microindentation stress-strain curves. These new protocols are first established in this paper and then demonstrated for Al-6061 by comparing the measured indentation stress-strain curves with the corresponding measurements from uniaxial tension tests. More specifically, the scaling factors between the uniaxial yield strength and the indentation yield strength was determined to be about 1.9, which is significantly lower than the value of 2.8 used commonly in literature. The reasons for this difference are discussed. Second, the benefits of these new protocols in facilitating high throughput exploration of process-property relationships are demonstrated through a simple case study. © 2016, The Author(s).
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页码:192 / 211
页数:19
相关论文
共 73 条
[1]  
Field J.S., Swain M.V., Determining the mechanical properties of small volumes of material from submicrometer spherical indentations, J Mater Res, 10, 1, pp. 101-112, (1995)
[2]  
Field J.S., Swain M.V., A simple predictive model for spherical indentation, J Mater Res, 8, 2, pp. 297-306, (1993)
[3]  
Basu S., Moseson A., Barsoum M.W., On the determination of spherical nanoindentation stress-strain curves, J Mater Res, 21, 10, pp. 2628-2637, (2006)
[4]  
Kalidindi S.R., Pathak S., Determination of the effective zero-point and the extraction of spherical nanoindentation stress-strain curves, Acta Mater, 56, 14, pp. 3523-3532, (2008)
[5]  
Herbert E.G., Et al., On the measurement of stress-strain curves by spherical indentation, Thin Solid Films, 398, pp. 331-335, (2001)
[6]  
Pathak S., Et al., Studying grain boundary regions in polycrystalline materials using spherical nano-indentation and orientation imaging microscopy, J Mater Sci, 47, pp. 815-823, (2012)
[7]  
Pathak S., Et al., Measuring the dynamic mechanical response of hydrated mouse bone by nanoindentation, J Mech Behav Biomed Mater, 4, pp. 34-43, (2011)
[8]  
Pathak S., Et al., Importance of surface preparation on the nano-indentation stress-strain curves measured in metals, J Mater Res, 24, 3, pp. 1142-1155, (2009)
[9]  
Pathak S., Et al., Viscoelasticity and high buckling stress of dense carbon nanotube brushes, Carbon, 47, 8, pp. 1969-1976, (2009)
[10]  
Pathak S., Stojakovic D., Kalidindi S.R., Measurement of the local mechanical properties in polycrystalline samples using spherical nanoindentation and orientation imaging microscopy, Acta Mater, 57, 10, pp. 3020-3028, (2009)