A study of the synthesis of triazoles using microwave irradiation

被引：0
|
作者：
Kenneth A. Savin
Michael Robertson
Doug Gernert
Steven Green
Erik J. Hembre
Jessie Bishop
机构：
[1] Eli Lilly and Company,Lilly Research Laboratories
来源：
Molecular Diversity | 2003年 / 7卷
关键词：
[3+2] cycloaddition; flow-through reaction; microwave irradiation; montmorillonite (K-10) clay; triazole;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Herein we describe the conversion of a known [3+2] cycloaddition reaction between an azide and an acetylene from a thermally promoted reaction to a microwave assisted process. Modification of conditions including concentration, temperature, solvent type and time were investigated. This methodology study led us to use high concentration and high temperatures to achieve the desired fast reaction times and high yields.
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页码：171 / 174
页数：3
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