3-Ethoxy-2,2-bis(methoxy-NNO-azoxy)propan-1-ol. Synthesis and X-ray diffraction analysis

被引：0
作者：
I. N. Zyuzin
N. I. Golovina
D. B. Lempert
G. V. Shilov
机构：
[1] Russian Academy of Sciences,Institute of Problems of Chemical Physics
来源：
Russian Chemical Bulletin | 2010年 / 59卷
关键词：
azoxy compounds; oxymethylation; X-ray diffraction study;
D O I：
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学科分类号：
摘要：
Reaction of bis(methoxy-NNO-azoxy)methane with formaldehyde in ethanol gives 3-ethoxy-2,2-bis(methoxy-NNO-azoxy)propan-1-ol as a minor product along with target 2,2-bis(methoxy-NNO-azoxy)ethanol. The structure of the former was confirmed by the counter synthesis and X-ray diffraction analysis.
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页码：1925 / 1929
页数：4
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