Reaction of 4-amino-3-methylthio-5-oxo-6-R-4,5-dihydro-1,2,4-triazines with sulfonylacetic acid nitriles

被引：0

作者：

V. N. Britsun

I. M. Bazavova

A. N. Esipenko

M. O. Lozinskii

机构：

[1] Institute of Organic Chemistry, Ukraine National Academy of Sciences

来源：

Chemistry of Heterocyclic Compounds | 2003年 / 39卷 / 12期

关键词：

4-amino-3-methylthio-5-oxo-6-R-4,5-dihydro-1,2,4-triazines; 7-amino-3-R-8-(R′-sulfonyl)-1,4-dihydropyrazolo[5,1-c][1,2,4] triazin-4-ones; Arylsulfonylacetonitriles; Dinitriles of sulfonyldiacetic and methylenebis(sulfonylacetic) acids;

D O I：

10.1023/B:COHC.0000018340.15398.18

中图分类号：

学科分类号：

摘要：

The reactions of 4-amino-3-methylthio-5-oxo-6-R-4,5-dihydro-1,2,4-triazines with arylsulfonyl-acetonitriles and with dinitriles of sulfonyldiacetic acid and methylenebis(sulfonylacetic) acid have been studied. 7-Amino-3-R-8- (R′-sulfonyl)-1,4-dihydropyrazolo[5,1-c][1,2,4]triazin-4-ones have been synthesized and these are the first representatives of geminal sulfones in which the heterocyclic ring is bound directly to the sulfur atoms of the sulfonyl groups.

引用

页码：1623 / 1626

页数：3

共 10 条

[1] Mel'nikov N.N., Pesticides, (1987)
[2] Kishida M., Oota C., Natsume F., Tomita M., Ikeda O., Chem. Abstr., 128, (1998)
[3] Bazavova I.M., Britsun V.N., Esipenko A.N., Lozinskii M.O., Khim. Geterotsikl. Soedin., (2003)
[4] Neplyuev V.M., Bazavova I.M., Esipenko A.N., Lozinskii M.O., Zh. Org. Khim., 30, (1994)
[5] Dornow A., Pietsch H., Chem. Ber., 100, (1967)
[6] Bazavova I.M., Esipenko A.N., Neplyuev V.M., Lozinskii M.O., Zh. Org. Khim., 30, (1994)
[7] Neplyuev V.M., Bazavova I.M., Lozinskii M.O., Usp. Khim., 55, (1986)
[8] Troger J., Hille W., J. Prakt. Chem., 71, (1905)
[9] McCormic J.E., McElhinney R.S., J. Chem. Soc., (1972)
[10] Dornow A., Menzel H., Marx P., Chem. Ber., 97, (1964)

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