Five-membered 2,3-dioxo heterocycles: CVI. Acylation of substituted (Z)-2-[1,3,4,4a,5,10b-Hexahydrophenanthridin-6(2H)-ylidene]acetamide with aroylketenes. crystal and molecular structure of substituted N-{(Z)-2-[1,3,4,4a,5,10b-Hexahydrophenanthridin-6(2H)-ylidene]acetyl}acrylamide

被引：0

作者：

V. V. Konovalova

Yu. V. Shklyaev

P. A. Slepukhin

A. N. Maslivets

机构：

[1] Russian Academy of Sciences,Institute of Technical Chemistry, Ural Branch

[2] Russian Academy of Sciences,Postovskii Institute of Organic Synthesis, Ural Branch

[3] Perm State University,undefined

来源：

Russian Journal of Organic Chemistry | 2014年 / 50卷

关键词：

Acetamide; Enamine; Chloranil; Endocyclic Nitrogen Atom; Enamine Fragment;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

Aroylketenes generated by thermolysis of 6-aryl-2,2-dimethyl-4H-1,3-dioxin-4-ones reacted with (Z)-2-[4a,7,10-trimethyl-1,3,4,4a,5,10b-hexahydrophenanthridin-6(2H)-ylidene]acetamide to give (Z)-3-aryl-3-hydroxy-N-{(Z)-2-[4a,7,10-trimethyl-1,3,4,4a,5,10b-hexahydrophenanthridin-6(2H)-ylidene]acetyl}acrylamides whose structure was confirmed by X-ray analysis.

引用

页码：1357 / 1360

页数：3

共 18 条

[1] Five-membered 2,3-dioxo heterocycles: LXIX. Direct heterocyclization of [3,4-dihydroisoquinolin-1(2H)-ylidene]-acetamides with 5-arylfuran-2,3-diones. Crystalline and molecular structure of (3E,5Z)-3-[3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]-5-(2-oxo-2-phenylethylidene)pyrrolidine-2,4-dione
V. V. Khalturina
Yu. V. Shklyaev
Z. G. Aliev
A. N. Maslivets
Russian Journal of Organic Chemistry, 2010, 46 : 539 - 542
[2] Five-membered 2,3-dioxo heterocycles: LXIX. Direct heterocyclization of [3,4-dihydroisoquinolin-1(2H)-ylidene]-acetamides with 5-arylfuran-2,3-diones. Crystalline and molecular structure of (3E,5Z)-3-[3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]-5-(2-oxo-2-phenylethylidene)pyrrolidine-2,4-dione
Khalturina, V. V.
Shklyaev, Yu. V.
Aliev, Z. G.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2010, 46 (04) : 539 - 542
[3] Five-membered 2,3-dioxo heterocycles: LXIII. Cascade recyclization of isopropyl 2-(1-aryl-4,5-dioxo-2-phenyl-4,5-dihydro-1H-pyrrol-3-yl)-2-oxoacetates with cyclic enamines. Crystalline and molecular structure of 1′-benzyl-6′,6′-dimethyl-3-[(Z)-phenyl(phenylamino)methylidene]-6′,7′-dihydro-3H-spiro[furan-2,3′-indole]-2′,4,4′,5(1′H,5′H)-tetraone
P. S. Silaichev
Z. G. Aliev
A. N. Maslivets
Russian Journal of Organic Chemistry, 2009, 45 : 126 - 130
[4] Five-membered 2,3-dioxo heterocycles: LXIII. Cascade recyclization of isopropyl 2-(1-aryl-4,5-dioxo-2-phenyl-4,5-dihydro-1H-pyrrol-3-yl)-2-oxoacetates with cyclic enamines. Crystalline and molecular structure of 1′-benzyl-6′,6′-dimethyl-3-[(Z)-phenyl(phenylamino)methylidene]-6′,7′-dihydro-3H-spiro[furan-2,3′-indole]-2′,4,4′,5(1′H,5′H)-tetraone
Silaichev, P. S.
Aliev, Z. G.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2009, 45 (01) : 126 - 130
[5] Five-membered dioxo heterocycles: CIV. Reaction of methyl 1-aryl-3-benzoyl-4,5-dioxo-4,5-dihydro-1H-pyrrole-2-carboxylates with cyclic enehydrazines. Crystal and molecular structure of N-[3′-benzoyl-1′-(4-chlorophenyl)-4′-hydroxy-6,6-dimethyl-2,4,5′-trioxo-1′,4,5,5′,6,7-hexahydrospiro-[indole-3,2′-pyrrol]-1(2H)-yl]benzamide
E. S. Denislamova
Z. G. Aliev
A. N. Maslivets
Russian Journal of Organic Chemistry, 2014, 50 : 1012 - 1016
[6] Five-membered dioxo heterocycles: CIV. Reaction of methyl 1-aryl-3-benzoyl-4,5-dioxo-4,5-dihydro-1H-pyrrole-2-carboxylates with cyclic enehydrazines. Crystal and molecular structure of N-[3'-benzoyl-1'-(4-chlorophenyl)-4'-hydroxy-6,6-dimethyl-2,4,5'-trioxo-1',4,5,5',6,7-hexahydrospiro-[indole-3,2'-pyrrol]-1(2H)-yl]benzamide
Denislamova, E. S.
Aliev, Z. G.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2014, 50 (07) : 1012 - 1016
[7] Five-membered dioxoheterocycles: XCIX. Reaction of 1-aryl-4-aroyl-5-methoxycarbonyl-1H-pyrrole-2,3-diones with indoles. Crystal and molecular structure of substituted 2-(indol-3-yl)pyrrole
E. S. Denislamova
P. A. Slepukhin
A. N. Maslivets
Russian Journal of Organic Chemistry, 2014, 50 : 225 - 228
[8] Five-Membered 2,3-dioxoheterocycles: XCV. Recyclization of 4-benzoyl-5-phenylfuran-2,3-dione at the action of substituted 1,3,3-trimethyl-2-azaspiro[4.5]dec-1-enes. Crystal and molecular structure of substituted 5-(2-azaspiro[4.5]dec-1-ylidene)cyclopent-3-ene-1,2-dione
Konovalova, V. V.
Shklyaev, Yu. V.
Slepukhin, P. A.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2013, 49 (11) : 1628 - 1631
[9] Five-membered 2,3-dioxo heterocycles: LXX. Spiro heterocyclization of 1H-pyrrole-2,3-diones by the action of 1,5-binucleophiles. Crystalline and molecular structure of ethyl 1′-benzyl-7-methoxy-3,3-dimethyl-1,2′-dioxo-5′-phenyl-1′,2,2′,3,4,10-hexahydro-1H-spiro[acridine-9,3′-pyrrole]-4′-carboxylate
P. S. Silaichev
M. V. Dmitriev
Z. G. Aliev
A. N. Maslivets
Russian Journal of Organic Chemistry, 2010, 46 : 1173 - 1177
[10] Five-Membered 2,3-Dioxo Heterocycles: LXX. Spiro Heterocyclization of 1H-Pyrrole-2,3-diones by the Action of 1,5-Binucleophiles. Crystalline and Molecular Structure of Ethyl 1′-Benzyl-7-methoxy-3,3-dimethyl-1,2′-dioxo-5′-phenyl-1′,2,2′,3,4,10-hexahydro-1H-spiro[acridine-9,3′-pyrrole]-4′-carboxylate
Silaichev, P. S.
Dmitriev, M. V.
Aliev, Z. G.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2010, 46 (08) : 1173 - 1177

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