Synthesis and spectral characterization of some new azo dyes and their metal complexes

被引：0
|
作者：
Rafet Kılınçarslan
Emin Erdem
Hasan Kocaokutgen
机构：
[1] Pamukkale University,Department of Chemistry
[2] Ondokuz Mayıs University,Department of Chemistry
来源：
Transition Metal Chemistry | 2007年 / 32卷
关键词：
Azobenzene; Complex Yield; Crude Precipitate; Magnetic Susceptibility Technique;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
A series of azo-metal chelate dyes have been synthesized by coupling substituted o-nitroaniline and p-t-/s-butylphenol. The spectral characterization of the azo dyes containing o-hydroxy group and azo-metal(II) chelate [metal(II): Cu, Ni, Co] dyes by IR spectra, UV–VIS spectra, NMR spectra, elemental analysis and magnetic susceptibility techniques are reported. The stoichiometry of the azo-metal chelates was determined by the spectroscopic titration method to be 1:2 (ML2).
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页码：102 / 106
页数：4
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