Synthesis and characterization of CdS and CdSe nanoparticles prepared from novel intramolecularly stabilized single-source precursors

被引:0
作者
Karuppasamy Kandasamy
Harkesh B. Singh
Shailendra K. Kulshreshtha
机构
[1] Indian Institute of Technology Bombay,Department of Chemistry
[2] Bhabha Atomic Research Center,Novel Materials and Structural Chemistry Division
来源
Journal of Chemical Sciences | 2009年 / 121卷
关键词
Nanoparticle; CdSe; CdS; TEM; XRD; SEM; hexagonal phase;
D O I
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中图分类号
学科分类号
摘要
In this note we describe the synthesis of cadmium sulphide and selenide nanoparticles from the corresponding novel single source precursors, M[E(Ox)]2 [E = S (1), Se (2); M = Cd; Ox = 2-(4,4-dimethyl-2-oxazolinyl)benzene] by thermolysing in tri-n-octylphosphine oxide (TOPO) at 280 °C, and their characterization by X-ray powder diffraction (XRD), transmission electron microscope (TEM) and scanning electron microscope (SEM) studies.
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页码:293 / 296
页数:3
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