One-pot synthesis of functionalized thioureas by reaction of benzoyl isothiocyanates, secondary amines, and alkyl propiolates

被引：0
|
作者：
Issa Yavari
S. Zahra Sayyed-Alangi
Maryam Sabbaghan
Rahimeh Hajinasiri
Nasir Iravani
机构：
[1] Islamic Azad University,Chemistry Department, Science and Research Campus
[2] Tarbiat Modares University,Chemistry Department
来源：
Monatshefte für Chemie - Chemical Monthly | 2008年 / 139卷
关键词：
Benzoyl isothiocyanate; Activated acetylenes; Secondary amines; Triphenylphosphine; Three-component reaction.;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
An efficient one-pot synthesis of functionalized thioureas is described via three-component reaction of benzoyl isothiocyanates, secondary amines, and alkyl propiolates in the presence of triphenylphosphine (20 mol%).
引用
收藏
页码：1025 / 1028
页数：3
相关论文
共 50 条
  • [1] One-pot synthesis of functionalized thioureas by reaction of benzoyl isothiocyanates, secondary amines, and alkyl propiolates
    Yavari, Issa
    Sayyed-Alangi, S. Zahra
    Sabbaghan, Maryam
    Hajinasiri, Rahimeh
    Iravani, Nasir
    MONATSHEFTE FUR CHEMIE, 2008, 139 (09): : 1025 - 1028
  • [2] Four-component one-pot synthesis of functionalized ynamines from reaction of benzoyl chlorides, secondary amines, acetylenic esters and ammonium thiocyanate
    Yavari, Issa
    Sabbaghan, Maryam
    Hosseim, Nargess
    Hossaini, Zinatossadat
    SYNLETT, 2007, (20) : 3172 - 3174
  • [3] Reaction between alkyl isocyanides and dialkyl acetylenedicarboxylates in the presence of benzoyl cyanides: one-pot synthesis of highly functionalized iminolactones
    Teimouri, MB
    Shaabani, A
    Bazhrang, R
    TETRAHEDRON, 2006, 62 (08) : 1845 - 1848
  • [4] ONE-POT SYNTHESIS OF ISOTHIOCYANATES FROM PRIMARY AMINES SYNTHESIS USING CYANAMIDE
    YAMAMOTO, T
    SUGIYAMA, S
    AKIMOTO, K
    HAYASHI, K
    ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 1992, 24 (03) : 346 - 349
  • [5] One-Pot Synthesis of Isothiocyanates from Amines Mediated by Carbon Tetrabromide
    Techapanalai, Saharat
    Annuur, Rose Malina
    Sukwattanasinitt, Mongkol
    Wacharasindhu, Sumrit
    CHEMISTRYSELECT, 2023, 8 (26):
  • [6] A One-Pot Approach to Pyridyl Isothiocyanates from Amines
    Zhang, Hao
    Liu, Rui-Quan
    Liu, Ke-Chang
    Li, Qi-Bo
    Li, Qing-Yang
    Liu, Shang-Zhong
    MOLECULES, 2014, 19 (09) : 13631 - 13642
  • [7] Synthesis of Isothiocyanates by Reaction of Amines with Phenyl Chlorothionoformate via One-Pot or Two-Step Process
    Li, Zheng-Yi
    Ma, Hong-Zhao
    Han, Chen
    Xi, Hai-Tao
    Meng, Qi
    Chen, Xin
    Sun, Xiao-Qiang
    SYNTHESIS-STUTTGART, 2013, 45 (12): : 1667 - 1674
  • [8] A one-pot, solid-phase synthesis of secondary amines from reactive alkyl halides and an alkyl azide
    Ayesa, Susana
    Samuelsson, Bertil
    Classon, Bjorn
    SYNLETT, 2008, (01) : 97 - 99
  • [9] Simple one-pot synthesis of thioureas from amines, carbon disulfide and oxidants in water
    Milosavljevic, Milutin M.
    Vukicevic, Ivan M.
    Drmanic, Sasa Z.
    Nikolic, Jasmina B.
    Marinkovic, Aleksandar D.
    Krstic, Sanja S.
    Petrovic, Slobodan D.
    JOURNAL OF THE SERBIAN CHEMICAL SOCIETY, 2016, 81 (03) : 219 - 231
  • [10] TRANSIMINATION - CONVERSION OF NITRILES INTO SECONDARY-AMINES IN A ONE-POT REACTION
    BRUSSEE, J
    VANDERGEN, A
    RECUEIL DES TRAVAUX CHIMIQUES DES PAYS-BAS-JOURNAL OF THE ROYAL NETHERLANDS CHEMICAL SOCIETY, 1991, 110 (01): : 25 - 26
12345