Structure refinement of cadmium cerium(IV) phosphate Cd0.5Ce2(PO4)3

被引：0
|
作者：
M. P. Orlova
D. B. Kitaev
M. L. Spiridonova
N. V. Zubkova
Yu. K. Kabalov
A. I. Orlova
机构：
[1] Nizhni Novgorod State University,Faculty of Chemistry
[2] Moscow State University,Faculty of Geology
来源：
Crystallography Reports | 2005年 / 50卷
关键词：
Radiation; Precipitation; Cadmium; Sample Preparation; Oxygen Atom;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Cadmium cerium orthophosphate Cd0.5Ce2(PO4)3 is synthesized by precipitation from aqueous solutions. The structure refinement from powder X-ray diffraction data is preceded by the sample preparation and structure solution. The refinement is carried out by the Rietveld method (ADP-2 diffractometer, CuKα radiation, Ni filter, 15° < 2θ < 120°, 2θ-scan step 0.02°, counting time 10 s per step). All calculations are carried out using the WYRIET program (version 3.3) within the sp. gr. P21/n. The structure is refined with anisotropic displacement parameters for cations and isotropic displacement parameters for oxygen atoms.
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页码：918 / 922
页数：4
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