Preparation of highly stable TiO2 sols and nanocrystalline TiO2 films via a low temperature sol–gel route

被引：2
作者：
Akash Katoch
Hohyeong Kim
Taejin Hwang
Sang Sub Kim
机构：
[1] Inha University,School of Materials Science and Engineering
[2] Korea Institute of Industrial Technology,Surface Technology and Heat Treatment R&D Division
来源：
Journal of Sol-Gel Science and Technology | 2012年 / 61卷
关键词：
Nanocrystalline TiO; film; Sol–gel; Low temperature deposition; Stable TiO; sol;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Highly stable TiO2 sols were prepared by adjusting the water-to-titanium molar ratio to ~4 in the process of hydrolysis and condensation of titanium isopropoxide in ethanol with HNO3. Particularly, long-term stable TiO2 sols were prepared without adding any chemical additives. Anatase TiO2 nanocrystallites with sizes of 3–5 nm in diameter were uniformly dispersed in the stable sol. Crystallized TiO2 films were successfully deposited on Si (100) using the stable sol via a dip-coating process with low temperature curing at as low as 100 °C. The synthesized TiO2 sols and films are promising for use in flexible or dye-sensitized solar cells.
引用
收藏
页码：77 / 82
页数：5
相关论文
共 50 条
  • [21] Preparation of SiO2/TiO2 and TiO2/TiO2 micropattern and their effects on platelet adhesion and endothelial cell regulation
    Li, Jing-an
    Yang, Ping
    Zhang, Kun
    Ren, Hui-lan
    Huang, Nan
    NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 2013, 307 : 575 - 579
  • [22] Preparation and characterization of TiO2 sols and their UV-cured hybrid thin films on plastic substrates
    Chao-Ching Chang
    Liao-Ping Cheng
    Chia-Ying Lin
    Yang-Yen Yu
    Journal of Sol-Gel Science and Technology, 2012, 63 : 30 - 35
  • [23] Characterization and photoactivity of TiO2 sols prepared with triethylamine
    Yu, Junxia
    Wang, Jingyu
    Zhang, Jian
    He, Zhike
    Liu, Zhihong
    Ai, Xinping
    MATERIALS LETTERS, 2007, 61 (28) : 4984 - 4988
  • [24] Photocatalytic and photoelectrochemical properties of sol-gel TiO2 films of controlled thickness and porosity
    Krysa, Josef
    Baudys, Michal
    Zlamal, Martin
    Krysova, Hana
    Morozova, Magda
    Kluson, Petr
    CATALYSIS TODAY, 2014, 230 : 2 - 7
  • [25] Optical constants of sol-gel derived TiO2 films characterized by spectroscopic ellipsometry
    Wang Xiao-Dong
    Shen Jun
    Wang Sheng-Zhao
    Zhang Zhi-Hua
    ACTA PHYSICA SINICA, 2009, 58 (11) : 8027 - 8032
  • [26] Annealing Temperature Effect on Nanostructured TiO2 Films
    Affendi, I. H. H.
    Sarah, M. S. P.
    Rusop, M.
    2014 IEEE INTERNATIONAL CONFERENCE ON SEMICONDUCTOR ELECTRONICS (ICSE), 2014, : 400 - 403
  • [27] Preparation of Mesoporous TiO2 Spheres via Sol-Gel Assisted Hydrothermal Method Using Double Templates
    Wang Dianping
    Liu Shouxin
    CHINESE JOURNAL OF CATALYSIS, 2012, 33 (10) : 1681 - 1688
  • [28] Crack formation in TiO2 films prepared by sol-gel processing:: Quantification and characterization
    Bockmeyer, Matthias
    Loebmann, Peer
    THIN SOLID FILMS, 2007, 515 (13) : 5212 - 5219
  • [29] The influence of "small molecules" on properties of TiO2 films prepared by sol-gel method
    Pagacova, J.
    Plsko, A.
    Michalkova, K.
    Sulcova, J.
    Bielikova, B.
    Tomagova, M.
    JOURNAL OF NON-CRYSTALLINE SOLIDS, 2014, 401 : 164 - 168
  • [30] Electrodeposition and characterization of nanocrystalline cuprous oxide thin films on TiO2 films
    Tang, YW
    Chen, ZG
    Jia, ZJ
    Zhang, LS
    Li, JL
    MATERIALS LETTERS, 2005, 59 (04) : 434 - 438
12345