Effect of Fe2O3 Nano-Oxide Addition on the Superconducting Properties of the (Bi,Pb)-2223 Phase

被引:0
作者
M. Roumié
S. Marhaba
R. Awad
M. Kork
I. Hassan
R. Mawassi
机构
[1] CNRS,Accelerator Laboratory, Lebanese Atomic Energy Commission
[2] Beirut Arab University,Physics Department, Faculty of Science
[3] Alexandria University,Physics Department, Faculty of Science
[4] Beirut Arab University,Physics Department, Faculty of Science
来源
Journal of Superconductivity and Novel Magnetism | 2014年 / 27卷
关键词
(Bi,Pb)-2223; Nano-Fe; O; Microstructure; PIXE; RBS;
D O I
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摘要
The effect of different weight percentages of nano-Fe2O3 on the properties of Bi1.8Pb0⋅4Sr2Ca2Cu3O10+δ superconducting phase was studied. Phase formation, elemental real contents and granular microstructure of the investigated samples were carried out using X-Ray powder Diffraction (XRD), Energy Dispersive X-ray emission (EDX), Proton Induced X-ray Emission (PIXE), Rutherford Backscattering Spectrometry (RBS) and Scanning Electron Microscopy (SEM). XRD data indicated that the volume fraction of (Bi,Pb)-2223 decreased as nano-Fe2O3 wt.% increased. PIXE and EDX analyses showed that the PIXE technique is more accurate for detecting the nano-Fe2O3 than the EDX technique. The oxygen content, determined from RBS, decreased as nano-Fe2O3 wt.% increased.
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页码:143 / 153
页数:10
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