Simultaneous LC Analysis of Aloe-Emodin, Rhein, Emodin, and Chrysophanol in Rhizoma Rhei-Type Preparations

被引：0

作者：

Ping Ren

Feng Qin

Xi Huang

Zhengyan Zhu

机构：

[1] Central South University,Laboratory of Ethnopharmacology, Institute of Integrated Traditional Medicine and Western Medicine, Xiangya Hospital

[2] Central South University,Key Unit of Traditional Chinese Medicine Gan of SATCM, Xiangya Hospital

[3] Central South University,Key Unit of the 11th Five

[4] Sichuan University,year Plan of SATCM in Cerebrosis, Xiangya Hospital

来源：

Chromatographia | 2009年 / 70卷

关键词：

Column liquid chromatography; Traditional Chinese medicine; Rhizoma Rhei; Anthraquinones;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

A simple and sensitive liquid chromatographic method has been established for simultaneous analysis of four compounds (aloe-emodin, rhein, emodin, and chrysophanol) in Rhizoma Rhei-type preparations. The compounds were separated in less than 20 min on a C18 column with 70:30 methanol–0.2% aqueous acetic acid as mobile phase at a flow rate of 1 mL min−1. The method was validated for specificity, accuracy, precision, and limits of detection. Good linear regression data (r2 > 0.9980) were obtained for all the calibration plots within the ranges tested. The method is an attractive alternative for evaluation of the quality of Rhizoma Rhei-type preparations.

引用

页码：1515 / 1517

页数：2

共 43 条

[11] Simultaneous HPTLC Determination of Rhein and Aloe-emodin in Senna alata Leaves from Thailand and their Commercial Products
Chewchinda, Savita
Sithisarn, Pongtip
NATURAL PRODUCT COMMUNICATIONS, 2017, 12 (03) : 399 - 401
[12] Pharmacodynamics of Five Anthraquinones (Aloe-emodin, Emodin, Rhein, Chysophanol, and Physcion) and Reciprocal Pharmacokinetic Interaction in Rats with Cerebral Ischemia
Li, Rong-Rong
Liu, Xue-Fang
Feng, Su-Xiang
Shu, Sheng-Nan
Wang, Pei-Yang
Zhang, Na
Li, Jian-Sheng
Qu, Ling-Bo
MOLECULES, 2019, 24 (10):
[13] Qualitative and quantitative analyses of aloe-emodin, rhein, and emodin in qi yin granules by high-performance thin-layer chromatography
Na Xi
Hongbing Liu
Shihao Xu
Xuehua Yan
JPC – Journal of Planar Chromatography – Modern TLC, 2020, 33 : 579 - 585
[14] Qualitative and quantitative analyses of aloe-emodin, rhein, and emodin in qi yin granules by high-performance thin-layer chromatography
Xi, Na
Liu, Hongbing
Xu, Shihao
Yan, Xuehua
JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC, 2020, 33 (06) : 579 - 585
[15] Antifungal Activity of Rhein and Aloe-Emodin from Rheum palmatum on Fish Pathogenic Saprolegnia sp
Yao, Jia-Yun
Lin, Ling-Yun
Yuan, Xue-Mei
Ying, Wen-Lin
Xu, Yang
Pan, Xiao-Yi
Hao, Gui-Jie
Shen, Jin-Yu
Wu, Jin-Chun
Ye, Ting
Ge, Pei-Hong
JOURNAL OF THE WORLD AQUACULTURE SOCIETY, 2017, 48 (01) : 137 - 144
[16] Analysis of the anthraquinones aloe-emodin and aloin by gas chromatography/mass spectrometry
ElSohly, MA
Gul, W
Murphy, TP
INTERNATIONAL IMMUNOPHARMACOLOGY, 2004, 4 (14) : 1739 - 1744
[17] Investigation on the binding of aloe-emodin with tyrosinase by spectral analysis and molecular docking
Zeng, Hua-jin
Liu, Zhe
Hu, Gui-zhou
Qu, Ling-bo
Yang, Ran
SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2019, 211 : 79 - 85
[18] Emodin, Aloe-emodin and Rhein Induced DNA Damage and Inhibited DNA Repair Gene Expression in SCC-4 Human Tongue Cancer Cells
Chen, Ya-Yin
Chiang, Su-Yin
Lin, Jaung-Geng
Yang, Jai-Sing
Ma, Yi-Shih
Liao, Ching-Lung
Lai, Tung-Yuan
Tang, Nou-Ying
Chung, Jing-Gung
ANTICANCER RESEARCH, 2010, 30 (03) : 945 - 951
[19] Analysis of the pharmacokinetics and metabolism of aloe-emodin following intravenous and oral administrations in rats
Yu, Chung-Ping
Shia, Chi-Sheng
Lin, Hui-Ju
Hsieh, Yow-Wen
Lin, Shiuan-Pey
Hou, Yu-Chi
BIOMEDICAL CHROMATOGRAPHY, 2016, 30 (10) : 1641 - 1647
[20] Electrochemical study of Aloe-emodin on an ionic liquid-type carbon paste electrode
Yan Wang
Huayu Xiong
Xiuhua Zhang
Shengfu Wang
Microchimica Acta, 2010, 169 : 255 - 260

← 1 2 3 4 5 →