Influence of the formation conditions of aluminophosphate gels on the morphology and pore structure of molecular sieve AlPO4-11

被引：0
|
作者：
M. R. Agliullin
V. V. Lazarev
B. I. Kutepov
机构：
[1] Russian Academy of Sciences,Institute of Petrochemistry and Catalysis
[2] Ufa Federal Research Center of the Russian Academy of Sciences,undefined
[3] Ufa State Aviation Technical University,undefined
来源：
Russian Chemical Bulletin | 2021年 / 70卷
关键词：
zeolites; aluminophosphate molecular sieve AlPO; -11; crystal morphology; micro-mesoporous materials;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Aluminophosphate gels were synthesized from aluminum isopropoxide, phosphoric acid, and di-n-propylamine. The influence of the synthesis conditions on the characteristics of gel crystallization products (samples of molecular sieve AlPO4-11) was studied using X-ray diffraction analysis, 27Al and 31P MAS NMR spectroscopy, Raman spectroscopy, scanning and transmission electron microscopy, and low-temperature nitrogen adsorption. The morphology of the crystals and secondary pore structure of molecular sieve AlPO4-11 can be controlled by changing the order of mixing of the starting components during synthesis of aluminophosphate gels.
引用
收藏
页码：47 / 55
页数：8
相关论文
共 50 条
  • [31] Synthesis and characterization of AlPO4-36: A novel aluminophosphate molecular sieve with ATS structure
    Department of Chemical Engineering, Laval University, Sainte-Foy, Que. G1K 7P4, Canada
    不详
    Microporous Mesoporous Mater, 3 (241-250):
  • [32] Investigations on the intrinsic and template-dependent transformations of AlPO4-11 molecular sieve under high pressure
    Chen, Shuanglong
    Li, Xin
    Yao, Zhen
    Dong, Enlai
    Shi, Lifen
    Du, Mingrun
    Yang, Xibao
    Liu, Ran
    Lv, Hang
    Liu, Bingbing
    MATERIALS CHEMISTRY AND PHYSICS, 2022, 292
  • [33] STRUCTURE DETERMINATION AND RIETVELD REFINEMENT OF ALUMINOPHOSPHATE MOLECULAR-SIEVE ALPO4-8
    RICHARDSON, JW
    VOGT, ETC
    ZEOLITES, 1992, 12 (01): : 13 - 19
  • [34] Intermediate Aluminophosphates as a Tool of Control over the Morphology and Secondary Porous Structure of AlPO4-11
    M. R. Agliullin
    B. I. Kutepov
    Petroleum Chemistry, 2021, 61 : 825 - 835
  • [35] 13C NMR of methane in an AlPO4-11 molecular sieve:: Exchange effects and shielding anisotropy
    Koskela, T
    Ylihautala, M
    Jokisaari, J
    Vaara, J
    PHYSICAL REVIEW B, 1998, 58 (22) : 14833 - 14836
  • [36] Morphology changes of transition-metal-substituted aluminophosphate molecular sieve AlPO4-5 crystals
    Tian, Dayong
    Yan, Wenfu
    Cao, Xuejing
    Yu, Jihono
    Xu, Ruren
    CHEMISTRY OF MATERIALS, 2008, 20 (06) : 2160 - 2164
  • [37] Simulation of alkane adsorption in the aluminophosphate molecular sieve AlPO4-5
    Maris, T
    Vlugt, TJH
    Smit, B
    JOURNAL OF PHYSICAL CHEMISTRY B, 1998, 102 (37): : 7183 - 7189
  • [38] Study on the thermal analysis of aluminophosphate molecular sieve AlPO4-12
    Ruilan, Zhao
    Hunan Shifan Daxue Ziran Kexue Xuebao/Natural Sciences Journal of Hunan Normal University, 1993, 16 (02):
  • [39] Intermediate Aluminophosphates as a Tool of Control over the Morphology and Secondary Porous Structure of AlPO4-11
    Agliullin, M. R.
    Kutepov, B. I.
    PETROLEUM CHEMISTRY, 2021, 61 (08) : 825 - 835
  • [40] Computational Study for Water Sorption in AlPO4-5 and AlPO4-11 Molecular Sieves
    Pillai, Renjith S.
    Jasra, Raksh V.
    LANGMUIR, 2010, 26 (03) : 1755 - 1764
12345