Influence of the formation conditions of aluminophosphate gels on the morphology and pore structure of molecular sieve AlPO4-11

被引：0
|
作者：
M. R. Agliullin
V. V. Lazarev
B. I. Kutepov
机构：
[1] Russian Academy of Sciences,Institute of Petrochemistry and Catalysis
[2] Ufa Federal Research Center of the Russian Academy of Sciences,undefined
[3] Ufa State Aviation Technical University,undefined
来源：
Russian Chemical Bulletin | 2021年 / 70卷
关键词：
zeolites; aluminophosphate molecular sieve AlPO; -11; crystal morphology; micro-mesoporous materials;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Aluminophosphate gels were synthesized from aluminum isopropoxide, phosphoric acid, and di-n-propylamine. The influence of the synthesis conditions on the characteristics of gel crystallization products (samples of molecular sieve AlPO4-11) was studied using X-ray diffraction analysis, 27Al and 31P MAS NMR spectroscopy, Raman spectroscopy, scanning and transmission electron microscopy, and low-temperature nitrogen adsorption. The morphology of the crystals and secondary pore structure of molecular sieve AlPO4-11 can be controlled by changing the order of mixing of the starting components during synthesis of aluminophosphate gels.
引用
收藏
页码：47 / 55
页数：8
相关论文
共 50 条
  • [21] Crystal morphology control of AlPO4-11 molecular sieves by microwave irradiation
    Chen, Yashao
    Luo, Xiaolin
    Chang, Pengmei
    Geng, Shouhua
    MATERIALS CHEMISTRY AND PHYSICS, 2009, 113 (2-3) : 899 - 904
  • [22] Key Stages in the Formation of AlPO4-11 via the Crystallization of a Boehmite-Based Aluminophosphate Gel
    M. R. Agliullin
    Z. R. Khairullina
    A. V. Faizullin
    A. I. Petrov
    A. A. Badretdinova
    V. P. Talzi
    B. I. Kutepov
    Catalysis in Industry, 2019, 11 : 87 - 94
  • [23] Key Stages in the Formation of AlPO4-11 via the Crystallization of a Boehmite-Based Aluminophosphate Gel
    Agliullin, M. R.
    Khairullina, Z. R.
    Faizullin, A., V
    Petrov, A., I
    Badretdinova, A. A.
    Talzi, V. P.
    Kutepov, B., I
    CATALYSIS IN INDUSTRY, 2019, 11 (02) : 87 - 94
  • [24] Synthesis of regularly shaped AlPO4-11 molecular sieve through a solid transformation approach
    Wang, Ping
    Wang, Congxin
    Lv, Guang
    Li, Peng
    Hou, Guangjin
    Qu, Wei
    Ma, Huaijun
    Wang, Donge
    Tian, Zhijian
    MICROPOROUS AND MESOPOROUS MATERIALS, 2020, 295
  • [25] On the synthesis of the aluminophosphate molecular sieve AlPO4-5
    Jahn, E., 1600, (09):
  • [26] Unusual bulky solvent molecule encapsulation in the organic-amine-occupied 10-membered ring channels of aluminophosphate molecular sieve AlPO4-11
    Guo, Junhui
    Wang, Chao
    Xu, Jun
    Deng, Feng
    Yan, Wenfu
    Shi, Wei
    Xu, Ruren
    INORGANIC CHEMISTRY COMMUNICATIONS, 2018, 88 : 6 - 10
  • [27] Characterization of the gel phases of AlPO4-11 molecular sieve synthesis by solid-state NMR
    Huang, YN
    Richer, R
    Kirby, CW
    JOURNAL OF PHYSICAL CHEMISTRY B, 2003, 107 (06): : 1326 - 1337
  • [28] Insight in the Crystallization Kinetics of AlPO4-11 Molecular Sieve Using Di-Isopropylamine as Template
    Mapele, Renilson O.
    Silva, Antonio O. S.
    Souza, Marcelo J. B.
    Pedrosa, Anne M. G.
    Coriolano, Ana C. F.
    Fernandes, Glauber J. T.
    Fernandes, Valter J., Jr.
    Araujo, Antonio S.
    APPLIED SCIENCES-BASEL, 2021, 11 (14):
  • [29] Sorption of water in aluminophosphate molecular sieve AlPO4-5
    Newalkar, BL
    Jasra, RV
    Kamath, V
    Bhat, SGT
    MICROPOROUS AND MESOPOROUS MATERIALS, 1998, 20 (1-3) : 129 - 137
  • [30] Synthesis and characterization of AlPO4-36:: a novel aluminophosphate molecular sieve with ATS structure
    Zahedi-Niaki, MH
    Xu, GY
    Meyer, H
    Fyfe, CA
    Kaliaguine, S
    MICROPOROUS AND MESOPOROUS MATERIALS, 1999, 32 (03) : 241 - 250
12345