Thermal, mechanical, and optical studies of NaBr-added l-alanine crystal

被引:0
|
作者
T. Jayanalina
G. Rajarajan
S. Parthiban
S. C. Mojumdar
机构
[1] KSR College of Engineering,Department of Physics
[2] Mahendra Engineering College,Department of Physics
[3] Annamalai University,Department of Chemistry, Faculty of Engineering and Technology
[4] University of Guelph,undefined
[5] Trencin University of A. Dubcek,undefined
来源
Journal of Thermal Analysis and Calorimetry | 2013年 / 112卷
关键词
Crystal growth; Amino acid crystals; Thermal studies; TG–DTA; FT-IR; XRD;
D O I
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中图分类号
学科分类号
摘要
The 1:1 adduct of l-Alanine and sodium bromide (l-ANaBr) crystal has been grown from aqueous solution by a slow evaporation technique. l-alanine and sodium bromide were used in the ratio 1:1 for synthesis. Characterizations were carried out to study the thermal, optical, and mechanical properties of the grown crystal. Single-crystal X- ray diffraction analysis shows that the grown crystal belongs to the monoclinic system. The crystalline nature and its various planes of reflections were observed by powder XRD analysis. Thermal studies reveal that the crystal is stable up to 113.37 °C. The chemical compositions of the grown crystal were determined by FT-IR spectral analysis. The transmittance, absorption, and reflection spectrum of l-ANaBr crystal studied using a UV–Vis spectrometer indicates that the crystal has good optical transparency. The mechanical property of the grown crystal studied using Vickers microhardness measurement reveals that the crystal is a soft material.
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页码:1025 / 1030
页数:5
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