Synthesis and crystal structure of 2-nitroxyethyl nicotinate and its complex with PdCl2

被引：0
作者：
B. S. Fedorov
N. I. Golovina
M. A. Fadeev
A. B. Eremeev
V. V. Arakcheeva
G. V. Strukov
V. V. Kedrov
G. V. Shilov
R. F. Trofimova
L. O. Atovmyan
机构：
[1] Russian Academy of Sciences,Institute of Chemical Physics in Chernogolovka
来源：
Russian Chemical Bulletin | 1998年 / 47卷
关键词：
nicotinoyl chloride; ethylene glycol mononitrate; 2-nitroxyethyl nicotinate, reaction with palladium(; ) chloride; -bis(2-nitroxyethyl nicotinate-; )dichloropalladium(; ), crystal structure, X-ray structural analysis;
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摘要：
The reaction of nicotinoyl chloride with ethylene glycol mononitrate yielded the previously unknown 2-nitroxyethyl nicotinate. The resulting ester was used as a ligand in the reaction with PdCl2 for preparing a new complex,trans-bis(2-nitroxyethyl nicotinate-N)dichloropalladium(ii). The structures of the ligand and the complex were established by X-ray structural analysis.
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页码：510 / 513
页数：3
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