Crystal structure of the bioctahedral cluster complex K6[Re12CS17(CN)6]·2CH3OH·10H2O

被引:0
作者
Yu. V. Mironov
S. -J. Kim
V. E. Fedorov
机构
[1] Russian Academy of Sciences,A. V. Nikolaev Institute of Inorganic Chemistry, Siberian Division
[2] Ewha Womans University,undefined
来源
Journal of Structural Chemistry | 2009年 / 50卷
关键词
rhenium; bioctahedral thiocyanate cluster; synthesis; crystal structure;
D O I
暂无
中图分类号
学科分类号
摘要
The cluster complex of K6[Re12CS17(CN)6]·2CH3OH·10H2O composition is separated by recrystallization of the K6[Re12CS17(CN)6]·20H2O compound from methanol. The compound crystallizes in hexagonal space group P-6m2 with unit cell parameters: a = 10.9932(14) Å, c = 14.631(4) Å, V = 1531.3(5) Å3, Z = 1, and dcalc = 3.720 g/cm3.
引用
收藏
页码:365 / 367
页数:2
相关论文
共 34 条
  • [1] Fedorov V. E.(2007)undefined Usp. Khim. 76 571-595
  • [2] Mironov Yu. V.(2001)undefined Chem. Rev. 101 2037-2066
  • [3] Naumov N. G.(1999)undefined J. Struct. Chem. 40 959-974
  • [4] Gabriel J.-C.(1998)undefined Chem. Commun. 17 1861-1862
  • [5] Boubekeur K.(1991)undefined Ukr. Khim. Zh. 57 675-680
  • [6] Uriel S.(1990)undefined Koordinats. Khim. 16 1062-1066
  • [7] Batail P.(1999)undefined Z. Anorg. Allg. Chem. 625 1212-1216
  • [8] Mironov Yu. V.(1991)undefined Angew. Chem. 103 1501-1503
  • [9] Fedorov V. E.(1995)undefined Inorg. Chem. 34 841-853
  • [10] Fedorov V. E.(2005)undefined Angew. Chem. Int. Ed. 44 6867-6871