Synthesis, crystal and molecular structure of 2-(3-chloropropyl)-6-methyl- 4-phenylquinazoline 3-oxide

被引：0

作者：

Kulikov O.V. ^{[1
]}

Mazepa A.V. ^{[1
]}

机构：

[1] A. B. Bogatsky Physico-Chemical Institute, National Academy of Sciences of Ukraine

来源：

Chemistry of Heterocyclic Compounds | 2007年 / 43卷 / 7期

关键词：

Mass spectrometry; Quinazoline; X-ray diffraction structural analysis;

D O I：

10.1007/s10593-007-0139-1

中图分类号：

学科分类号：

摘要：

The acylation of the syn isomer of the oxime of 2-amino-5- methylbenzophenone with 4-chlorobutyryl chloride gives a mixture of the anti isomer of the 4-chlorobutyryloximine of 2-(4-chlorobutyryl)amino-5- methylbenzophenone and 2-(3-chloropropyl)-6-methyl-4-phenylquinazoline 3-oxide. The crystal and molecular structure of this oxide was established by X-ray diffraction structural analysis. The molecule is planar. The electron impact fragmentation of 2-(3-chloropropyl)-6-methyl-4-phenylquinazoline 3-oxide was discussed. © 2007 Springer Science+Business Media, Inc.

引用

页码：879 / 886

页数：7

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