Mild and efficient silylation of alcohols under ambient and solvent-free conditions with phosphorus pentoxide supported on alumina (P2O5/Al2O3) as catalyst

被引:0
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作者
Hamid Reza Shaterian
Nafiseh Fahimi
Kobra Azizi
机构
[1] University of Sistan and Baluchestan, Department of Chemistry, Faculty of Sciences
来源
关键词
P; O; /Al; O; Trimethylsilylation; Hexamethyldisilazane; Alcohols; Solvent-free; Catalyst;
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摘要
P2O5/Al2O3, an easily handled recyclable catalyst, has been used in an eco-friendly and mild procedure for trimethylsilyl protection of alcohols by use of hexamethyldisilazane. Solvent-free, ambient reaction conditions, easy work-up, short reaction times, excellent yields and reusability of the catalyst are noticeable features of this method.
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页码:947 / 954
页数:7
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