Characterization of Thermal-Sprayed HAP and HAP/TiO2 Coatings for Biomedical Applications

被引:0
作者
Sarbjit Kaur
Niraj Bala
Charu Khosla
机构
[1] IKGPTU Kapurthala,Mechanical Engineering Department
[2] BBSBEC,Applied Sciences Department
[3] Chitkara University,undefined
来源
Journal of Thermal Spray Technology | 2018年 / 27卷
关键词
biomaterials; bond coat; Hank’s solution; HVFS; hydroxyapatite; simulated body fluid; surface roughness;
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中图分类号
学科分类号
摘要
In the present study, hydroxyapatite (HAP) coating along with HAP/TiO2 coating has been deposited by high-velocity flame spray (HVFS) technique onto 316LSS. Titania was used as a bond coat and HAP as top coat in HAP/TiO2 coating. The main aim of the study is to investigate the corrosion behavior of thermal spray coating of HAP and HAP/TiO2 on steel. Electrochemical corrosion testing was carried out using potentiodynamic polarization test. The corrosion behavior of bare and as-sprayed specimens was analyzed in simulated body fluid known as Hank’s solution. As-sprayed specimens along with corroded specimens were further characterized by XRD, SEM/EDS, and x-ray mapping analysis. It was observed that the HAP/TiO2 coating possessed higher microhardness (280 Hv) as compared to HAP coating (254 Hv). Surface roughness also got enhanced in case of HAP/TiO2 coating (9.35 μm) as compared to pure HAP coating (7.37 μm). The porosity of the HAP coating was found to be higher than the bond coating. It was observed that the Ca/P ratio almost resembled that of the natural bone composition. The corrosion resistance of steel increased after the deposition of HAP and HAP/TiO2 coatings. The maximum corrosion resistance was exhibited by HAP/TiO2 coating.
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页码:1356 / 1370
页数:14
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