Synthesis of 2,2,5,7-tetramethyl-1,3-diazaadamantan-6-one and study of the supramolecular structure of its monohydrate

被引：0
作者：
A. I. Dalinger
A. V. Medved’ko
M. A. Kalinin
V. A. Sereda
A. V. Churakov
S. Z. Vatsadze
机构：
[1] Lomonosov Moscow State University,Department of Chemistry
[2] Russian Academy of Sciences,N. D. Zelinsky Institute of Organic Chemistry
[3] Russian Academy of Sciences,N. S. Kurnakov Institute of General and Inorganic Chemistry
来源：
Russian Chemical Bulletin | 2021年 / 70卷
关键词：
supramolecular chemistry; bispidines; aminals; 1,3-diazaadamantanones; X-ray diffraction; NMR spectra;
D O I：
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学科分类号：
摘要：
The reaction of 1,5-dimethyibispidin-9-one with acetone, acting as both a solvent and a reagent, affords 2,2,5,7-tetramethyl-1,3-diazaadamantan-6-one. The structure of the monohydrate of the target compound, which is a hydrogen-bonded supramolecular polymer, was determined by X-ray diffraction analysis.
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页码：1002 / 1005
页数：3
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