Structure of a deaza dimer of 4-methyl-3H-1,2,4-triazole-3,5(4H)-dione

被引：0
|
作者：
Simon G. Bott
Alan P. Marchand
Kaipenchery A. Kumar
Dongxia Xing
机构：
[1] University of Houston,Department of Chemistry
[2] University of North Texas,Department of Chemistry
来源：
Journal of Chemical Crystallography | 1999年 / 29卷
关键词：
Crystal structure; dimer; triazole;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
The title compound crystallizes in the monoclinic space group, P21/n; a = 9.0024(5), b = 5.8135(3), c = 15.2232(8) Å, β = 91.153(4)° Z = 4; and R = 0.050 based on 853 observed, unique reflections. The structure consists of two fused five-membered triazole rings, oriented relative to each other at 152°.
引用
收藏
页码：15 / 18
页数：3
相关论文
共 50 条
  • [21] 4-Amino-5-(2-hydroxyphenyl)-2H-1,2,4-triazole-3(4H)-thione
    Dinçer, M
    Özdemir, N
    Çetin, A
    Cansiz, A
    Sekerci, M
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O3214 - O3216
  • [22] 4-Ethyl-5-(2-hydroxyphenyl)-2H-1,2,4-triazole-3(4H)-thione
    Dege, N
    Özdemir, N
    Çetin, A
    Cansiz, A
    Sekerci, M
    Dinçer, M
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O17 - O19
  • [23] A NEW SYNTHETIC ROUTE TO 5-SUBSTITUTED-2H-1,2,4-TRIAZOLE-3(4H)-THIONES
    Begum, T. Shalina
    Muneer, C. P.
    Shafi, P. M.
    INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 2013, 22 (03) : 297 - 300
  • [24] 2,2'-(4-Methyl-4H-1,2,4-triazole-3,5-diyl)-dibenzenesulfonamide
    Akhtar, Tasleem
    Siddiqui, Waseeq Ahmad
    Ashraf, Adnan
    Tahir, M. Nawaz
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O754 - U2398
  • [25] Synthesis, characterization and crystal structure of the dimeric silver(I) complex containing 4-amino-5-methyl-2H-1,2,4-triazole-3(4H)-thione
    Sharafi, T
    Heravi, MM
    Ghassemzadeh, M
    Neumüller, B
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2005, 631 (12): : 2297 - 2299
  • [26] 5-[(1H-1,2,4-yriazol-1-yl)methyl]-4-(4-fluorobenzylideneamino)-2H-1,2,4-triazole-3(4H)-thione
    Yang, XY
    Shang, YQ
    Yu, GP
    Zhang, PY
    Li, WH
    Hou, BR
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O3371 - O3372
  • [27] ABNORMAL DIELS-ALDER REACTION OF OXAZOLES WITH 4-PHENYL-3H-1,2,4-TRIAZOLE-3,5(4H)-DIONE AND DIETHYL AZODICARBOXYLATE, AND X-RAY CRYSTAL-STRUCTURE OF AN ADDUCT
    IBATA, T
    SUGA, H
    ISOGAMI, Y
    TAMURA, H
    SHI, XL
    BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1992, 65 (11) : 2998 - 3007
  • [28] Synthesis, characterization and crystal structure of a silver(I) complex containing AMTT - (AMTT=4-amino-5-methyl-2H-1,2,4-triazole-3(4H)-thione)
    Yazdanbakhsh, Mohammad
    Hakimi, Mohammad
    Heravi, Majid M.
    Boese, Roland
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2006, 632 (14): : 2201 - 2203
  • [29] ABNORMAL DIELS-ALDER REACTION OF 5-ALKOXYTHIAZOLES WITH HIGHLY REACTIVE DIENOPHILES - 4-PHENYL-3H-1,2,4-TRIAZOLE-3,5(4H)-DIONE, DIETHYL AZODICARBOXYLATE, AND DIETHYL OXOMALONATE
    SHI, XL
    IBATA, T
    SUGA, H
    MATSUMOTO, K
    BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1992, 65 (12) : 3315 - 3321
  • [30] ANALOGS OF NUCLEOSIDES .33. 4-BETA-D-RIBOFURANOSYL-1,2,4-TRIAZIN-3,5(2H,4H)-DIONE AND 4-BETA-D-RIBOFURANOSYL-6-METHYL-1,2,4-TRIAZIN--3,5(2H,4H)-DIONE
    HREBABECKY, H
    COLLECTION OF CZECHOSLOVAK CHEMICAL COMMUNICATIONS, 1982, 47 (03) : 994 - 999
12345