Facile synthesis of micron-sized thiol-functional polysilsesquioxane microspheres through a one-step sol-gel method

被引：0
|
作者：
Lu Han
Zhenyu Nie
Rongsheng Gao
Chengyou Kan
机构：
[1] Tsinghua University,Department of Chemical Engineering and Key Laboratory of Advanced Materials of Ministry of Education
来源：
Journal of Sol-Gel Science and Technology | 2024年 / 109卷
关键词：
Polysilsesquioxane; Micron-sized microsphere; One-step method; Sol-gel method; Thiol-functionalization;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Micron-sized TPMs are prepared by a one-step base-catalyzed method in the presence of PVP.Monodisperse small TPMs with a Dmean of about 4 μm are synthesized without stirring by nucleation and growth.Large TPMs with a Dmean larger than 10 μm are formed due to the coalescence of oligomer droplets with stirring.
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页码：330 / 345
页数：15
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