Synthesis of 3-(3-alkyl-5-thioxo-1H-4,5-dihydro-1,2,4-triazol-4-yl) aminocarbonylchromones

被引：0

作者：

Cao L. ^{[1
]}

Zhang L. ^{[1
,3
]}

Cui P. ^{[1
,3
]}

机构：

[1] Coll. of Chem. and Chem. Engineering, Xinjiang University

[2] , S.

[3] Coll. of Chem. and Chem. Engineering, Xinjiang University, Urumqi 830046, P. R. China

来源：

Chemistry of Heterocyclic Compounds | 2004年 / 40卷 / 5期

关键词：

3-(3-alkyl-5-thioxo-1H-4,5-dihydro-1,2,4-triazol-4-yl) aminocarbonylchromones; 3-formylchromone; synthesis;

D O I：

10.1023/B:COHC.0000037320.27881.27

中图分类号：

学科分类号：

摘要：

A series of 3-(3-alkyl-5-thioxo-1H-4,5-dihydro-1,2,4-triazol-4-yl) aminocarbonylchromones has been prepared by oxidation of 3-formylchromone with Jones' reagent followed by reaction with 3-alkyl-4-amino-4,5-dihydro-1,2,4- triazole-5(1H)-thione in the presence of POCl 3. The structures of the compounds were confirmed by IR, LC-MS, and 1H NMR spectra and elemental analyses.

引用

页码：635 / 640

页数：5

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