Synergistic effect of resorcarene and cyclodextrin mixed stationary phase in gas chromatography

被引:0
作者
D. -Q. Xiao
Y. Ling
Y. -X. Wen
R. -N. Fu
J. -L. Gu
R. -J. Dai
A. -Q. Luo
机构
[1] Beijing Institute of Technology,Department of Chemical Engineering
来源
Chromatographia | 1997年 / 46卷
关键词
Gas chromatography; Mixed stationary phase; Resourcarene; Cyclodextrin;
D O I
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中图分类号
学科分类号
摘要
A new resorcarene derivatives, ethylhexylresorcarene, was synthesized and used as stationary phase in opentubular (capillary) columns. It was combined with heptakis(2,6-di-O-pentyl-3-O-trifluoroacetyl)-β-CD and coated on fused-silica capillary tubes. By studying the chromatographic properties of the mixed stationary phase and its selectivity for different isomers, as well as comparing with the resorcarene and the CD used as individual stationary phases, a synergistic effect was observed on the mixed stationary phase.
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页码:177 / 182
页数:5
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