Nickel(II) hexamethyleneiminedithiocarbamate complexes with triphenylphosphine or tributylphosphine

被引：0
作者：
Marek Pavlíček
Zdeněk Trávníček
Richard Pastorek
Jaromír Marek
机构：
[1] Palacký University,Department of Inorganic and Physical Chemistry
[2] Masaryk University,X
来源：
Transition Metal Chemistry | 2003年 / 28卷
关键词：
Spectroscopy; Physical Chemistry; Nickel; Inorganic Chemistry; Catalysis;
D O I：
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学科分类号：
摘要：
A series of square-planar nickel(II) hexamethylenedithiocarbamate complexes with heterogeneous coordination spheres of composition [NiX(hmidtc)Y] · nCHCl3 [X = Cl, Br, I or NCS; hmi = C6H12, dtc = S2CN−; Y = PPh3 or PBu3, n = 0,1] have been synthesized and characterized by elemental analyses, i.r. and u.v.–v.i.s. spectroscopy, magnetochemical and conductivity measurements, and by thermal analysis. X-ray structures of [NiCl(hmidtc)(PPh3)] · CHCl3 and [NiBr(hmidtc)(PPh3)] · CHCl3 have been determined.
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页码：260 / 264
页数：4
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