Lanthanum Hexaboride Production by Borothermal Reduction – an Investigation

被引：0

作者：

E. N. Kablov

N. E. Shchegoleva

Yu. E. Lebedeva

P. L. Zhuravleva

M. L. Vaganova

A. S. Chainikova

机构：

[1] All-Russian Research Institute at National Research Center Kurchatov Institute (NRC Kurchatov Institute – VIAM),

来源：

Glass and Ceramics | 2023年 / 80卷

关键词：

lanthanum hexaboride; rare-earth metal borides; spark plasma sintering; boride synthesis; borothermal reduction; carbothermal reduction;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

The processes involved in obtaining lanthanum hexaboride by boron thermal reduction using heat-treatment in a vacuum furnace and spark plasma sintering were investigated. Single-phase powder of lanthanum hexaboride was obtained at 1800 – 1900°C with excess boron content in the batch mix equal to 20 wt%. Spark plasma sintering allows the synthesis temperature of the single-phase lanthanum hexaboride powder to be lowered to 1700 and 1600°C with excess boron content 10 and 20 wt.%, respectively, in the batch.

引用

页码：58 / 69

页数：11

共 30 条

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