Study of thermal behavior of α-PbO2, using TG and DSC

被引：0
|
作者：
Sajadi S.A.A. [1 ]
Alamolhoda A.A. [1 ]
Hashemian S.J. [1 ]
机构：
[1] Sharif University of Technology, Institute of Water and Energy, Tehran
来源：
Journal of Thermal Analysis and Calorimetry | 2008年 / 92卷 / 3期
关键词：
DSC; Lead(IV) oxide; TG; Thermal analysis; XRD;
D O I：
10.1007/s10973-007-8687-2
中图分类号：
学科分类号：
摘要：
Using two techniques of thermogravimetry and differential scanning calorimetry under O2 gas atmosphere from 25 to 600°C, the thermal behavior of laboratory-produced compound lead(IV) oxide α-PbO2 was investigated. The identity of products at different stages were confirmed by XRD technique. Both techniques produced similar results supporting the same decomposition stages for the compound. Three distinct energy changes were observed, namely, two endothermic and one exothermic in DSC. The amount of ΔH for each peak is also reported. © 2008 Springer Science+Business Media, LLC.
引用
收藏
页码：917 / 920
页数：3
相关论文
共 50 条
  • [1] Study of thermal behavior of α-PbO2, using TG and DSC
    Alamlhoda, A. A.
    Sajadi, S. A. A.
    Hashemian, S. J.
    JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, 2008, 92 (03) : 917 - 920
  • [2] Study of thermal behavior of CrO3 using TG and DSC
    Sajadi, S. A. A.
    Khaleghian, M.
    JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, 2014, 116 (02) : 915 - 921
  • [3] Study of thermal behavior of CrO3 using TG and DSC
    S. A. A. Sajadi
    M. Khaleghian
    Journal of Thermal Analysis and Calorimetry, 2014, 116 : 915 - 921
  • [4] Investigation of thermal behavior of Heliotropiumindicum L. lyophilized extract by TG and DSC
    Russany Silva da Costa
    Charles Alberto Brito Negrão
    Sarah Regina Pereira Camelo
    Roseane Maria Ribeiro-Costa
    Wagner Luiz Ramos Barbosa
    Carlos Emmerson Ferreira da Costa
    José Otávio Carréra Silva Júnior
    Journal of Thermal Analysis and Calorimetry, 2013, 111 : 1959 - 1964
  • [5] TG and DSC as tools to analyse the thermal behaviour of EVA copolymers
    Diez, E.
    Rodriguez, A.
    Gomez, J. M.
    Galan, J.
    JOURNAL OF ELASTOMERS AND PLASTICS, 2021, 53 (07) : 792 - 805
  • [6] Thermal characterization of indinavir sulfate using TG, DSC and DSC-photovisual
    Rosali Maria Ferreira da Silva
    Flávia Patrícia Morais de Medeiros
    T. G. Nascimento
    R. O. Macêdo
    P. J. R. Neto
    Journal of Thermal Analysis and Calorimetry, 2009, 95 : 965 - 968
  • [7] THERMAL CHARACTERIZATION OF INDINAVIR SULFATE USING TG, DSC AND DSC-PHOTOVISUAL
    Ferreira da Silva, Rosali Maria
    Morais de Medeiros, Flavia Patricia
    Nascimento, T. G.
    Macedo, R. O.
    Neto, P. J. R.
    JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, 2009, 95 (03) : 965 - 968
  • [8] Investigation of thermal behavior of Heliotropium indicum L. lyophilized extract by TG and DSC
    da Costa, Russany Silva
    Brito Negrao, Charles Alberto
    Pereira Camelo, Sarah Regina
    Ribeiro-Costa, Roseane Maria
    Ramos Barbosa, Wagner Luiz
    Ferreira da Costa, Carlos Emmerson
    Carrera Silva Junior, Jose Otavio
    JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, 2013, 111 (03) : 1959 - 1964
  • [9] Thermal reactions of polyethylene with coal (TG/DSC approach)
    P. Straka
    J. Náhunková
    Journal of Thermal Analysis and Calorimetry, 2004, 76 : 49 - 53
  • [10] Thermal reactions of polyethylene with coal (TG/DSC approach)
    Straka, P
    Náhunková, J
    JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, 2004, 76 (01) : 49 - 53
12345