Synthesis and structure of complex compound Rh(III) of (NH4)2[Rh(NO2)3(NH3)(µ-OH)]2 composition

被引：0
|
作者：
S. P. Khranenko
I. A. Baidina
S. A. Gromilov
机构：
[1] Russian Academy of Sciences,A. V. Nikolayev Institute of Inorganic Chemistsry, Siberian Division
来源：
Journal of Structural Chemistry | 2006年 / 47卷
关键词：
rhodium; X-ray phase analysis; X-ray diffraction analysis; crystallochemistry;
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学科分类号：
摘要：
The crystalline structure of a new compound Rh(III) of (NH4)2[Rh(NO2)3(NH3)(µ-OH)]2 composition has been determined. The crystallographic characteristics are H16N10O14Rh2: a = 6.3963(2) Å, b = 9.3701(4) Å, c = 13.6646(5) Å, β = 102.266(1)°, V = 800.28(5) Å3, Z = 2, dcalc = 2.432 g/cm3. The distance Rh...Rh in the dimer is 3.200 Å.
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页码：375 / 379
页数：4
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