Immuno-affinity columns versus conventional clean-up: a method-comparison study for the determination of zearalenone in corn

被引：0

作者：

R. Schuhmacher

R. Krska

M. Grasserbauer

W. Edinger

H. Lew

机构：

[1] Institute for Agrobiotechnology (IFA-Tulln),

[2] Center for Analytical Chemistry,undefined

[3] Konrad Lorenz Straße 20,undefined

[4] A-3430 Tulln,undefined

[5] Austria,undefined

[6] Federal Office of Agrobiology,undefined

[7] Wieningerstraße 8,undefined

[8] 4025 Linz,undefined

[9] Austria,undefined

来源：

Fresenius' Journal of Analytical Chemistry | 1998年 / 360卷

关键词：

Analytical Data; Corn; Performance Characteristic; Good Correspondence; Zearalenone;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

The efficiency of a modern analytical method employing immuno-affinity columns (IACs) is compared to a well established traditional technique with respect to the determination of zearalenone (ZON) in corn in the μg/kg range. Despite of a constant error of about 4 μg/kg in the examined working range of 10–200 μg/kg, analytical data obtained from the analysis of spiked and naturally contaminated samples showed good correspondence for the compared methods. The performance characteristics of immuno-affinity-chromatography as a new clean-up technique for the determination of ZON in corn is reported for the first time and compared to a conventional clean-up procedure

引用

页码：241 / 245

页数：4

共 18 条

[1] Immuno-affinity columns versus conventional clean-up: a method-comparison study for the determination of zearalenone in corn
Schuhmacher, R
Krska, R
Grasserbauer, M
Edinger, W
Lew, H
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1998, 360 (02): : 241 - 245
[2] Determination of Sudan I by high performance liquid chromatography with immuno-affinity column clean-up
Zhu, Lixin
Meng, Wei
Qiu, Xuemei
Liu, Renrong
Xu, Ling
Xu, Fuyong
ADVANCES IN CHEMICAL ENGINEERING III, PTS 1-4, 2013, 781-784 : 1694 - 1699
[3] Determination of zearalenone in corn by means of immunoaffinity clean-up and high-performance liquid chromatography with fluorescence detection
J Chromatogr, 1 (133-140):
[4] Determination of zearalenone in corn by means of immunoaffinity clean-up and high-performance liquid chromatography with fluorescence detection
Visconti, A
Pascale, M
JOURNAL OF CHROMATOGRAPHY A, 1998, 815 (01) : 133 - 140
[5] Optimization of the determination of deoxynivalenol in corn samples by liquid chromatography and a comparison of two clean-up principles
Abramovic, B
Jajic, I
Juric, V
Gaál, FF
JOURNAL OF THE SERBIAN CHEMICAL SOCIETY, 2005, 70 (07) : 1005 - 1013
[6] Development of a selective sample clean-up method based on immuno-ultrafiltration for the determination of deoxynivalenol in maize
Boehm, Christina
Cichna-Markl, Margit
Brenn-Struckhofova, Zdenka
Razzazi-Fazeli, Ebrahim
JOURNAL OF CHROMATOGRAPHY A, 2008, 1202 (02) : 111 - 117
[7] BSA-based sample clean-up columns for ochratoxin A determination in wine: Method development and validation
Leal, Tania
Abrunhosa, Luis
Domingues, Lucilia
Venancio, Armando
Oliveira, Carla
FOOD CHEMISTRY, 2019, 300
[8] A collaborative study of an HPLC method for determination of ochratoxin A in wheat using immunoaffinity column clean-up
Scudamore, KA
MacDonald, SJ
FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT, 1998, 15 (04): : 401 - 410
[9] Comparison of extraction and clean-up procedures for analysis of zearalenone in corn, rice and wheat grains by high-performance liquid chromatography with photodiode array and fluorescence detection
Llorens, A
Mateo, R
Mateo, JJ
Jiménez, M
FOOD ADDITIVES AND CONTAMINANTS, 2002, 19 (03): : 272 - 281
[10] Study on CC/MS (SIM) for determination of carbamate and organonitrogen pesticides in foods with simple clean-up by SPE method
Kawasaki, M
Inoue, T
Fukuhara, K
Uchiyama, S
JOURNAL OF THE FOOD HYGIENIC SOCIETY OF JAPAN, 1999, 40 (05): : 382 - 390

← 1 2 →