Electrochemical Synthesis of 2,5-Dichloroaniline

被引：0

作者：

V. R. Islamgulova

A. P. Tomilov

S. G. Akhmerova

V. T. Gil'mkhanova

Yu. E. Sapozhnikov

机构：

[1] Research and Technological Institute of Herbicides and Plant Growth Regulators,

[2] State Research Institute of Organic Chemistry and Technology,undefined

来源：

Russian Journal of Applied Chemistry | 2003年 / 76卷

关键词：

Sulfate; Sulfuric Acid; Acid Concentration; Cathode Material; Target Product;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

A procedure was proposed for electrochemical reduction of 2,5-dichloronitrobenzene to 2,5-dichloroaniline in aqueous-ethanolic solution of sulfuric acid. The procedure for preparing 2,5-dichloroanilinium sulfate was optimized. The influence exerted by the cathode material, nature and amount of the organic solvent, sulfuric acid concentration, and electrolysis temperature on the yield and quality of the target product was discussed.

引用

页码：1076 / 1078

页数：2