Determination of Trace Iron in KH2PO4 Crystal by Derivative Adsorption Chronopotentiometry

被引:0
作者
Xiaoli Zhang
Chong Tian
Nan Zhang
Yunfang Zhao
机构
[1] Shandong University,Department of Chemistry and Chemical Engineering
来源
Microchimica Acta | 2004年 / 148卷
关键词
Key words: Iron; Eriochrome blue black R (EBBR); chronopotentiometry.;
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摘要
A sensitive derivative adsorption chronopotentiometric method was developed to determine trace amounts of Fe3+. The influence of preconcentration time, pH of solution and constant reducing current of the peak height is discussed. The detection limit and the linear range are 5.0 × 10−10 and 2.0 × 10−9∼3.0 × 10−6 mol L−1, respectively. The method was used to determine trace Fe3+ in KH2PO4 crystals (KDP).
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页码:55 / 58
页数:3
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