Synthesis of 5,6-O-Cyclohexylidene-1-amino-3-azahexane and Its Co(II), Ni(II), Cu(II) Complexes

被引：0
作者：
O. F. Ozturk
M. Sekerci
E. Ozdemir
机构：
[1] Canakkale Onsekiz Mart University,Faculty of Arts and Sciences, Chemistry Department
[2] Firat University,Faculty of Arts and Sciences, Chemistry Department
来源：
Russian Journal of Coordination Chemistry | 2005年 / 31卷
关键词：
Spectroscopy; Acetate; Physical Chemistry; Inorganic Chemistry; Magnetic Susceptibility;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
5,6-O-Cyclohexylidene-1-amino-3-azahexane (L) is synthesized from 1-chloro-2,3-O-cyclohexylidenepropane, which is prepared by the reaction between epichlorohydrin and cyclohexanone. In this reaction, BF3 · OEt2 is used as a catalyst. Complexes of Co(II), Ni(II) and Cu(II) acetates with this ligand are prepared. The structures of the ligand and its complexes are proposed based on elemental analysis, IR and UV-VIS spectroscopy, magnetic susceptibility, conductometry, and 1H and 13C NMR spectroscopy.
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页码：651 / 654
页数：3
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