Solid phase extraction of uranium(VI) on phosphorus-containing polymer grafted 4-aminoantipyrine

被引：0
作者：
Mustafa Soylak
Mansoor Khan
Rasim Alosmanov
Jasmin Shah
Mohammad Rasul Jan
机构：
[1] Erciyes University,Faculty of Sciences, Department of Chemistry
[2] University of Peshawar,Institute of Chemical Sciences
[3] Baku State University,Chemistry Department
来源：
Journal of Radioanalytical and Nuclear Chemistry | 2016年 / 308卷
关键词：
Solid phase extraction; Spectrophotometry; Determination; Uranium; Arsenazo(III);
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Phosphorus-containing polymer grafted 4-aminoantipyrine has been synthesized and used for solid phase extraction of U(VI) prior to its UV–Visible spectrophotometric determination by using arsenazo(III). The adsorbent was characterized by using FT-IR and SEM analysis. The influence of parameters including pH, adsorbent dose, amount of complexing reagent, sample volume and matrix effect have been optimized. The detection limit was determined as 1.4 µg L−1 with preconcentration factor of 30 and RSD of 1.4 %. The accuracy was checked by the analysis of GBW07424 soil and TMDA-64.2 environmental water certified reference materials. The method was applied to natural water and soil samples.
引用
收藏
页码：955 / 963
页数：8
相关论文
共 187 条
[1]  
Donia AM(2009)Removal of uranium(VI) from aqueous solutions using glycidyl methacrylate chelating resins Hydrometall 95 183-189
[2]  
Atia AA(2009)Removal of uranium (VI) from aqueous solution by adsorption of hematite J Environ Radioact 100 162-166
[3]  
Moussa EMM(2015)Application of bimodal distribution to the detection of changes in uranium concentration in drinking water collected by random daytime sampling method from a large water supply zone Chemosphere 138 377-382
[4]  
El-Sherif AM(1997)Determination of molybdenum and uranium in biological materials by radiochemical neutron activation analysis J Radioanal Nucl Chem 216 51-57
[5]  
Abd El-Magied MO(1983)Gamma-ray spectrometric determination of uranium-series nuclides in marine phosphorites Anal Chem 55 1796-1800
[6]  
Shuibo X(2006)Electrochemical transient techniques for determination of uranium and rare-earth metal separation coefficients in molten salts Electrochim Acta 51 2463-2470
[7]  
Chun Z(1979)Laser-induced fluorescence for the direct determination of small concentrations of uranium in water Microchim Acta 72 159-170
[8]  
Xinghuo Z(2003)Synthesis of novel chitosan resin derivatized with serine moiety for the column collection/concentration of uranium and the determination of uranium by ICP-MS Anal Chim Acta 480 239-249
[9]  
Jing Y(2013)Development of an extractive spectrophotometric method for uranium using MWCNTs as solid phase and arsenazo(III) as chromophore J Radioanal Nucl Chem 296 1239-1245
[10]  
Xiaojian Z(2013)Room temperature ionic liquid-based dispersive liquid–liquid microextraction of uranium in water samples before spectrophotometric determination Anal Methods 5 5260-5266
12345678910