Sonochemical Synthesis of One-Dimensional Nano-structure of Three-Dimensional Cadmium(II) Coordination Polymer

被引：0
|
作者：
Gholam Hossein Shahverdizadeh
Ali Morsali
机构：
[1] Islamic Azad Univrsity,Research Laboratory, Department of Applied Chemistry
[2] Faculty of Sciences,Department of Chemistry
[3] Tarbiat Modares University,undefined
来源：
Journal of Inorganic and Organometallic Polymers and Materials | 2011年 / 21卷
关键词：
Nano-structure; Coordination polymer; Cadmium(II);
D O I：
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学科分类号：
摘要：
Nano-wires and nano-rods of a new three-dimensional cadmium(II) coordination polymer, {[Cd3(3-pyc)4(NCS)2(H2O)4]·2H2O}n (1); 3-Hpyc = 3-pyridinecarboxilic acid, were synthesized by a sonochemical method in two different concetrations. The morphology of the nano-structures depend strongly on reactants’ concentration. The new nano-structures were characterized by scanning electron microscopy, X-ray powder diffraction, elemental analyses and IR spectroscopy. Compound 1 was structurally characterized by single-crystal X-ray diffraction and is a three-dimensional polymer with two types of Cd(II) coordination environments.
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页码：694 / 699
页数：5
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