The state of the matter and urgency of milk whey recovery have been analyzed. The well-founded need for various combinations of processes for the purpose of obtaining optimal conditions is shown. The material balance of the main elements of ash and protein is presented. Methods for optimizing the electrophysical processing of milk whey and the characteristics of major technological parameters have been determined. Optimal conditions and anodic liquid compositions, as well as the type of diaphragm, have been selected. The aims of the further investigations for the full and wasteless recovery of milk whey for obtaining high quality products have been preset.