Analysis of Micronutrients and Heavy Metals in Portuguese Infant Milk Powders by Wavelength Dispersive X-ray Fluorescence Spectrometry (WDXRF)

被引:0
作者
Tânia A. P. Fernandes
José A. A. Brito
Luísa M. L. Gonçalves
机构
[1] Instituto Superior de Ciências da Saúde Egas Moniz,Centro de Investigação Interdisciplinar Egas Moniz (CiiEM)
[2] Campus Universitário,undefined
来源
Food Analytical Methods | 2015年 / 8卷
关键词
Infant milk powders; Mineral nutrients; Heavy metals; WDXRF;
D O I
暂无
中图分类号
学科分类号
摘要
Concentrations of trace mineral nutrients such as Cu, Fe, and Zn have been analyzed by WDXRF in eight different infant milk powders, representing the majority of the milk powder brands commercialized in Portuguese pharmacies. Results suggest that the concentrations of some of elements analyzed are not consistent with the values labeled by manufacturers. However, all fall inside the concentration ranges defined by the Portuguese and European legislations, except for Al. The presence of aluminum was detected in all analyzed formulations in an average concentration of 8.25 to 19.75 mg Kg−1. This study also reveals the feasibility of WDXRF for the quantitative analysis of trace mineral nutrients in milk powder samples. Moreover, the approach described herein, using the WDXRF technique in helium mode, presents a new methodological advantage over similar published studies. This technique may represent an option for quality control of milk powder formulations, particularly at their production site.
引用
收藏
页码:52 / 57
页数:5
相关论文
共 77 条
[1]  
Abernethy DR(2010)Metal impurities in food and drugs Pharm Res 27 750-755
[2]  
Destefano AJ(2009)Advisability of X-ray fluorescence analysis of dry residue of cow milk applied to monitor environment X- Ray Spectrometry 39 22-27
[3]  
Cecil TL(2009)Maternal milk concentration of Zinc, Iron, Selenium, and Iodine and its relationship to dietary intakes Biol Trace Elem Res 127 6-15
[4]  
Zaidi K(2002)Levels of 26 elements in infant formula from USA, UK, and Nigeria by microwave digestion and ICP-OES Food Chem 77 439-447
[5]  
Williams RL(2007)Determination of major and minor elements in dairy products through inductively coupled plasma optical emission spectrometry after wet partial digestion and neutron activation analysis Food Chem 100 390-395
[6]  
Gunicheva TN(2008)Sample preparation for the determination of metals in food samples using spectroanalytical methods - A Review Appl Spectrosc Rev 43 67-92
[7]  
Hannan MA(2010)Mineral and nutritional analysis of Polish infant formulas J Food Compos Anal 23 424-431
[8]  
Faraji B(2009)Micronutrient transfer: infant absorption Adv Exp Med Biol 639 29-40
[9]  
Tanguma J(2009)Determination of metal residues in active pharmaceutical ingredients according to European current legislation by using X-ray fluorescence spectrometry J Anal At Spectrom 24 1253-1257
[10]  
Longoria N(2003)Aluminium content of Spanish infant formula Food Addit Contam 20 470-481