Effect of Pre-carbonization Temperature on the Properties of Plasticized Spinning Polyacrylonitrile Fibers

被引:0
作者
Xiang Li
Zhaoling Li
Xiaonan Dang
Dan Luan
Feng Wang
机构
[1] Zhenjiang College,Institute of Chemical and Materials Engineering
[2] Zhenjiang Key Laboratory of Functional Chemistry,Key Laboratory of Textile Science and Technology, Ministry of Education, College of Textiles
[3] Donghua University,undefined
[4] Zhenjiang Entry - Exit Inspection and Quarantine Bureau,undefined
来源
Fibers and Polymers | 2018年 / 19卷
关键词
Plasticized spinning; Properties; Pre-carbonization; Reaction;
D O I
暂无
中图分类号
学科分类号
摘要
In this work, plasticized spinning PAN fibers were treated at low carbonization temperature for the first time. The properties of treated fibers were characterized by elemental analysis (EA), scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FTIR) respectively. The SEM results show that cross section of the pre-carbonized fibers is circular with no apparent skin-core structure. During the pre-carbonization process (320-380°C), fracture mode of the fibers gradually changes from ductile to brittle and fibril diameter gradually decreases. Pre-carbonization temperature at 350°C significantly accelerates chemical reactions. The FTIR results show that a stable oxygen structure is generated as treated at 320°C.
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页码:692 / 696
页数:4
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