Facile synthesis of new (Z)-6-arylmethylidene-1,3,4-thiadiazin-5(6H)-one derivatives

被引:0
|
作者
N. H. Metwally
F. M. Abdelrazek
A. Jaeger
机构
[1] Cairo University,Institute of Organic Chemistry
[2] Technical University of Dresden,undefined
来源
Chemistry of Heterocyclic Compounds | 2013年 / 48卷
关键词
'-arylacetonitrilimines; (; )-6-arylmethylidene-1,3,4-thiadiazin-5(6; )-one derivatives; 3-aryl-2-sulfanylpropenoic acids;
D O I
暂无
中图分类号
学科分类号
摘要
3-Aryl-2-sulfanylpropenoic acids reacted with acetohydrazonyl chlorides in refluxing absolute ethanol in the presence of equimolar amounts of triethylamine, forming (Z)-6-arylmethylidene-1,3,4-thiadiazin-5-one derivatives. X-ray study on the crystal of one of the obtained products was carried out.
引用
收藏
页码:1696 / 1700
页数:4
相关论文
共 50 条
  • [1] Facile synthesis of new (Z)-6-arylmethylidene-1,3,4-thiadiazin-5(6H)-one derivatives
    Metwally, N. H.
    Abdelrazek, F. M.
    Jaeger, A.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2013, 48 (11) : 1696 - 1700
  • [2] Syntheses and structures of new substituted 4-aryl-sulfonyl-4H-1,3,4-thiadiazin-5(6H)-ones
    Jia, GF
    Li, ZM
    HETEROATOM CHEMISTRY, 1997, 8 (01) : 71 - 76
  • [4] SYNTHESIS AND STRUCTURE OF 4-PHENYL-1,3,4,4H-THIADIAZIN-5(6H)-ONE
    MATSUBARA, Y
    YOSHIHARA, M
    NAKANURA, T
    YAMADA, S
    MAESHIMA, T
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1983, 16 (1-2): : 89 - 96
  • [5] Synthesis, in vitro Antimicrobial, and Cytotoxic Activities of New 1,3,4-Oxadiazin-5(6H)-one Derivatives from Dehydroabietic Acid
    Jin, Xiao-Yan
    Zhang, Kang-Ping
    Chen, Hao
    Miao, Ting-Ting
    Wang, Shi-Fa
    Gu, Wen
    JOURNAL OF THE CHINESE CHEMICAL SOCIETY, 2018, 65 (05) : 538 - 547
  • [6] THE CHEMISTRY OF A 1,3,4-THIADIAZIN-6-ONE
    BAYDAR, AE
    BOYD, GV
    LINDLEY, PF
    JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1981, (19) : 1003 - 1004
  • [7] ON REACTIONS OF THIADIAZINONES: SYNTHESIS OF NEW 6-ARYLIDENE-1,3,4-THIADIAZIN-5-ONES
    Dalloul, Hany M.
    El-Shorafa, Ali Z.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2009, 45 (06) : 735 - 741
  • [8] On reactions of thiadiazinones: synthesis of new 6-arylidene-1,3,4-thiadiazin-5-ones
    Hany M. Dalloul
    Ali Z. El-Shorafa
    Chemistry of Heterocyclic Compounds, 2009, 45 : 735 - 741
  • [9] One-pot synthesis and fungicidal activities of derivatives of imidazo[2,1-b]-1,3,4-thiadiazol-5(6H)-one
    Sun, Yong
    Fu, Bo-Qiao
    Ding, Ming-Wu
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2006, 181 (06) : 1437 - 1443
  • [10] Synthesis of 4H-cyclopenta[c]furan-5(6H)-one derivatives
    Tu, Xianxia
    Peng, Haiyun
    Deng, Guisheng
    TETRAHEDRON, 2020, 76 (35)