A Zr(IV)-based porphyrinic metal-organic framework as a solid-phase sorbent for extraction of sulfonamides prior to their quantitation by LC-MS

被引：0
作者：
Ze-Hui Deng
Gui-Ju Xu
Xiao-Li Wang
Xia Wang
Ming-Lin Wang
Jin-Ming Lin
Ru-Song Zhao
机构：
[1] Qilu University of Technology (Shandong Academy of Sciences),Key Laboratory for Applied Technology of Sophisticated Analytical Instruments of Shandong Province, Shandong Analysis and Test Center
[2] Shandong Agricultural University,College of Food Science and Engineering
[3] Tsinghua University,Department of Chemistry
来源：
Microchimica Acta | 2018年 / 185卷
关键词：
Nanoparticles; PCN-224; Absorption; Pretreatment; Antibiotics; Food samples; Water samples;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
A porphyrinic metal–organic framework (PCN-224) was fabricated and used as an adsorbent for solid-phase extraction of ultratrace levels of polar sulfonamide antibiotics from food and drinking waters. The PCN-224 was characterized by scanning electron microscopy, Fourier transform infrared spectroscopy, and powder X-ray diffraction analyses. Parameters affecting the extraction efficiency were optimized. The sulfonamides were quantified by liquid chromatography-tandem mass spectrometry. Figures of merit include (a) low limits of detection (0.07–0.47 ng·L−1), (b) wide linear ranges (0.5–2000 ng·L−1), and (c) good repeatabilities (2.8%–6.7%) and reproducibilities (1.7%–5.1%). The method was successfully applied to the determination of sulfonamides in food and drinking water samples.
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