Synthesis of 3-amino-4-methyl-6-trifluoromethylthieno[2,3-b]pyridine-2-carboxanilide and its crystal and molecular structure

被引：0

作者：

K. G. Nikishin

V. N. Nesterov

V. P. Kislyi

A. M. Shestopalov

V. V. Semenov

机构：

[1] Russian Academy of Sciences,N. D. Zelinsky Institute of Organic Chemistry

[2] Russian Academy of Sciences,A. N. Nesmeyanov Institute of Organoelement Compounds

来源：

Russian Chemical Bulletin | 1998年 / 47卷

关键词：

cyanothioacetamide; 3-cyano-4-methyl-6-trifluoromethylpyridine-2(1; )-thione; 3-amino-4-methyl-6-trifluoromethylthieno[2,3-; ]pyridine-2-carboxanilide; X-ray anaysis;

D O I：

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中图分类号：

学科分类号：

摘要：

4-Methoxy-1,1,1-trifluoropent-3-en-2-one reacts with cyanothioacetamide to give 3-cyano-4-methyl-6-trifluoromethylpyridine-2(1H)-thione, which was transformed into 3-amino-4-methyl-6-trifluoromethylthieno[2,3-b]pyridine-2-carboxanilide by the reaction with chloroacetanilide. The crystal and molecular structure of the amide obtained was studied by X-ray analysis.

引用

页码：679 / 681

页数：2

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