A Comprehensive Assessment of All-Oleate Polysorbate 80: Free Fatty Acid Particle Formation, Interfacial Protection and Oxidative Degradation

被引:0
作者
Nidhi Doshi
Jamie Giddings
Lin Luis
Arthur Wu
Kyle Ritchie
Wenqiang Liu
Wayman Chan
Rosalynn Taing
Jeff Chu
Alavattam Sreedhara
Aadithya Kannan
Pervina Kei
Ian Shieh
Tobias Graf
Mark Hu
机构
[1] Pharmaceutical Development,
[2] Genentech Inc.,undefined
[3] Analytical Operations,undefined
[4] Genentech Inc.,undefined
[5] Pharma Technical Development Analytics,undefined
[6] Roche Diagnostics GmbH,undefined
来源
Pharmaceutical Research | 2021年 / 38卷
关键词
free fatty acids; monoclonal antibodies; polysorbate hydrolysis; polysorbate oxidation; visible particles;
D O I
暂无
中图分类号
学科分类号
摘要
引用
收藏
页码:531 / 548
页数:17
相关论文
共 278 条
[1]  
Dwivedi M(2018)Polysorbate degradation in biotherapeutic formulations: identification and discussion of current root causes Int J Pharm 552 422-436
[2]  
Blech M(2010)Adsorption behavior of a surfactant and a monoclonal antibody to sterilizing-grade filters J Pharm Sci 99 2620-2627
[3]  
Presser I(2008)Behaviour of polysorbate 20 during dialysis, concentration and filtration using membrane separation techniques J Pharm Sci 97 764-774
[4]  
Garidel P(1998)Tween protects recombinant human growth hormone against agitation-induced damage via hydrophobic interactions J Pharm Sci 87 1554-1559
[5]  
Mahler H-C(2008)Polysorbates 20 and 80 used in the formulation of protein biotherapeutics: structure and degradation pathways J Pharm Sci 97 2924-2935
[6]  
Huber F(2012)Analysis of polysorbate 80 and its related compounds by RP-HPLC with ELSD and MS detection J Chromatogr Sci 50 598-607
[7]  
Kishore RS(1997)Composition analysis of detergents of the polyoxyethylene type: comparison of thin-layer chromatography, reversed-phase chromatography and matrix-assisted laser desorption/ionization mass spectrometry J Chromatogr A 791 245-253
[8]  
Reindl J(2014)Characterization and stability study of polysorbate 20 in therapeutic monoclonal antibody formulation by multidimensional ultrahigh-performance liquid chromatography–charged aerosol detection–mass spectrometry Anal Chem 86 5150-5157
[9]  
Rückert P(2011)Mixed-mode and reversed-phase liquid chromatography–tandem mass spectrometry methodologies to study composition and base hydrolysis of polysorbate 20 and 80 J Chromatogr A 1218 2138-2145
[10]  
Müller R(2015)Understanding particle formation: solubility of free fatty acids as Polysorbate 20 degradation byproducts in therapeutic monoclonal antibody formulations Mol Pharm 12 3792-3804