Experimental study of phase transformation in non-equilibrium hypoeutectic alloy from the Fe–Cr–Ni–Mo–C system

被引:0
作者
K. Wieczerzak
P. Bała
G. Cios
T. Tokarski
K. Górecki
Ł. Frocisz
机构
[1] AGH University of Science and Technology,Faculty of Metals Engineering and Industrial Computer Science
[2] AGH University of Science and Technology,Academic Centre for Materials and Nanotechnology
来源
Journal of Thermal Analysis and Calorimetry | 2017年 / 127卷
关键词
Fe–Cr–Ni–Mo–C; Phase transformation; Dilatometry; DSC; Eutectic carbides;
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学科分类号
摘要
In the present study, experimental and thermodynamic analysis of phase transformation in hypoeutectic Fe–24Cr–11Ni–4Mo–0.64C alloy is presented. The investigated alloy was synthesized in an arc furnace in high-purity argon atmosphere using suction-casting unit. Chemical composition of the alloy was determined using an optical emission spectrometer. The microstructure was characterized by scanning electron microscopy. Phase composition in as-cast state was analysed by X-ray diffraction and compared with thermodynamic calculations for equilibrium state using Thermo-Calc software. The analysis of phase transformations was conducted by dilatometry and differential scanning calorimetry investigations. It was found that phase composition of the alloy after non-equilibrium solidification (cooling rate ~30 °C s−1) differs significantly from equilibrium state. Critical temperatures of phase transformations in the alloy were determined.
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页码:449 / 455
页数:6
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