1,10-Phenanthroline-2,9-dicarboxylic acid diamides: synthesis, structure, and solubility

被引：0
作者：
V. S. Petrov
N. A. Avagyan
P. S. Lamport
P. I. Matveev
M. V. Evsiunina
V. A. Roznyatovsky
B. N. Tarasevich
K. L. Isakovskaya
Yu. A. Ustynyuk
V. G. Nenajdenko
机构：
[1] Lomonosov Moscow State University,Department of Chemistry
[2] Russian Academy of Sciences,A. N. Nesmeyanov Institute of Organoelement Compounds
[3] Mendeleev University of Chemical Technology of Russia,undefined
来源：
Russian Chemical Bulletin | 2023年 / 72卷
关键词：
1,10-phenanthroline-2,9-dicarboxylic acid diamides; tetradentate ligand; alkylaryl-substituted ligand; solubility; NMR; X-ray analysis;
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摘要：
A wide range of 1,10-phenanthroline-2,9-dicarboxylic acid diamides was synthesized, differing in the structure of substituents in the amide function and in the nature of substituents at positions 4 and 7 of the heteroaromatic ring. All new compounds were characterized by NMR, IR spectroscopy, and high resolution mass spectrometry. The molecular structure of one of the ligands was unambiguously confirmed by X-ray diffraction analysis. The solubility of all the obtained compounds in 3-nitrobenzotrifluoride was quantitatively evaluated.
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页码：697 / 705
页数：8
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