The crystal and molecular structure of bis(melamine)silver(I) perchlorate, Ag(C3H6N6)2ClO4

被引：0
|
作者：
Haoguo Zhu
Zhi Yu
Xiaozeng You
Huaiming Hu
Xiaoying Huang
机构：
[1] Nanjing University,Coordination Chemistry Institute, State Key Laboratory of Coordination Chemistry
[2] Chinese Academy of Sciences,State Key Laboratory of Structural Chemistry, Fujian Institute of Research On the Structure of Matter
来源：
Journal of Chemical Crystallography | 1999年 / 29卷
关键词：
Ag(mela); ClO; hydrogen bond; weak bond;
D O I：
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中图分类号：
学科分类号：
摘要：
The crystal structure of the title compound, Ag(mela)2ClO4 (mela = melamine), has been investigated by X-ray diffraction techniques, the crystals are triclinic, space group P1¯, with a = 5.236(2), b = 7.5385(9) c = 19.063(3) Å, α = 99.91(1), β = 90.53(2), γ = 108.32(2)° and Z = 2. The Ag atom has a coordination geometry with two strong bonds (2.162(2) and 2.179(4) Å) to the nitrogen of the melamines and two weak bonds (2.776(4) and 2.785(4) Å) to oxygen atoms of the ClO−4anions. The N—Ag—N vector is markedly nonlinear (angle at Ag 167.7(2)°).
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页码：239 / 242
页数：3
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