X-Ray Diffraction Study of Crystal and Molecular Structures of Azo Compounds of Two β-Diketones

被引:0
作者
F. N. Bahmanova
Sh. A. Tahirli
R. K. Askerov
S. R. Hajiyeva
F. M. Chyragov
机构
[1] Baku State University,
[2] Lankaran State University,undefined
来源
Journal of Structural Chemistry | 2019年 / 60卷
关键词
β-diketone; synthesis of azo compounds; X-ray diffraction analysis; molecular packing; hydrogen bonding;
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摘要
Novel compounds 2-(2-(2-hydroxy-4-nitrophenyl) hydrazono)-1,3-diphenyl propane-1,3-dione and 2-(2-(2-hydroxy-4-nitrophenyl) hydrazono)-1-phenyl butane-1,3-dione are prepared on the base of β-diketones. Crystal and molecular structures of synthesized compounds are determined by X-ray diffraction analysis. The crystals are found to be monoclinic. The compounds are represented only by their hydrazo forms. The structural data for the two obtained compounds are compared with previously reported data.
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页码:1681 / 1687
页数:6
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